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• a 19 Striker Ave Ste 8 Sequoia Sacramento,CA 95834 (916)921.9600 Analytical FAX(916)921-0100 www.sequoialabscom Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County S308356 1326 N.Market Blvd. Project Number,791291/00003000 Reported: Sacramento CA,95834 Project Manager: Steve Giacomini 09/03/03 16:39 Anions by EPA Method 300.0-Quality Control Sequoia Analytical-Sacramento Reporting Spike Source °/,REC RPD Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes Batch 3080286-General Preparation Blank(3080286-BLKI) Prepared&Analyzed:08/20/03 Chloride ND 0,031 0.20 mg/l 0-09 Nitrate as N ND 0.0045 0.023 0-09 Nitrate as NO3 ND 0.056 0.10 0-09 Sulfate as SO4 ND 0.031 0.20 0-09 Laboratory Control Sample(3080286-BSI) Prepared&Analyzed:08/20/03 Chloride 5.64 0.03I 0.20 mg/l 5.00 113 80-120 0-09 Nitrate as N 1.34 0.0045 0.023 1.13 119 80-120 0-09 Nitrate as NO3 5.94 0.056 0.10 5.00 119 80-120 0-09 Sulfate as SO4 10.8 0.031 0.20 10.0 108 80-120 0-09 Matrix Spike(3080286-MSI) Source:S308356-01 Prepared&Analyzed:08/20/03 Chloride 243 0.31 2.0 mg/l 50.0 190 106 75-125 0-09 • Nitrate as N 16.5 0.045 0.23 11.3 2.8 121 75-125 0-09 Nitrate as NO3 73.2 0.56 1.0 50.0 13 120 75-125 0-09 Sulfate as SO4 541 0.31 2.0 100 440 101 75-125 0-09 Matrix Spike Dup(3080286-MSDI) Source:S308356-01 Prepared&Analyzed:08/20/03 Chloride 244 0.31 2.0 mg/l 50.0 190 108 75-125 0.4 20 0-09 Nitrate as N 16.5 0.045 0.23 11.3 2.8 121 75-125 0 20 0-09 Nitrate as NO3 73.1 0.56 1.01. 50.0 13 120 75-125 0.1 20 0-09 Sulfate as SO4 539 0.31 2.0 100 440 99 75-125 0.4 20 0-09 Sequoia Analytical-Sacramento The results In this report apply to the samples anal med in accordance with the chain of custody document.Unless otherwise stated,results are reported on a wet weight basis. This analytical report must be reproduced in Its entirety. tPage 16 of 17