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Sequay y 7.oi819 Striker Avenue.Suite 8 <br /> Sacramento,CA 95834 <br /> (916)921-9600 <br /> Analytical <br /> c s�l FAX(916)921-0400 <br /> j 1 a-1 La wwwsequotatabs.com <br /> Shaw E&I-Sacramento Project: Corral Hollow Landfill,San Joaquin County <br /> 1326 N.Market Blvd. Project Number: 791291100002000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 08/11/03 16:47 <br /> _ Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Sptke Source °/.REC RPD <br /> lAnalyte Result MDL Limit Units Level Result "/.REC Limits RPD Limit Notes <br /> Batch 3080090-EPA 5030B (P/T] <br /> Blank(3080090-BLKI) Prepared:08/07/03 Analyzed:08/08/03 <br /> Trichloroethene ND 0.36 0.50 ugfl <br /> Trichlorofluoromethane ND 0.42 .0.50 " <br /> 1,2,3-Trichloropropane ND 0.55 1.0 " <br /> 1,2,4-Trimethylbenzene ND 0.18 0.50 <br /> 1,3,5-Trimethylbenzene ND 0.28 0.50 " <br /> vinyl chloride ND 0.16 0.50 " <br /> Xylenes(total) ND 0.48 0.50 " <br /> Surrogate:Dibromofluoroinethane 24.6 25.0 98 70-130 <br /> Surrogate:1,2-DCA-d4 24.4 25.0 98 70-130 <br /> Surrogate:Toluene-d8 24,S 25.0 98 70-130 <br /> Surrogate:4-BFB 15.1 25.0 100 70-130 <br /> LCS(3080090-BSI) Prepared 08107/03 Analyzed:08/08/03 <br /> Benzene 23.7 0.28 0.50 ug/l 25.0 95 70-130 <br /> Chlorobenzene 23.7 0.32 0.50 25.0 95 70-130 <br /> 1,1-Dichloroethene 19.7 0.24 0.50 25.0 79 70-130 <br /> Toluene 23.6 0.32 0.50 25.0 94 70-130 <br /> Trichloroethene 20.6 0.36 0.50 25.0 82 70-130 <br /> Surrogate:Dibromofluoromethane 24.8 1S.0 99 70-130 <br /> Surrogate:1.2-DCA-d4 26.0 2S.0 104 70-130 <br /> Surrogate:Toluene-d8 24.2 2S.0 97 70-130 <br /> Surrogate.4-BFB 26.4 " 2S.0 106 70-130 <br /> Matrix Spike(3080090-MSJ) Source:S307585-02 Prepared:09107/03 Analyzed:08/08/03 <br /> Benzene 23.7 0.28 0.50 ug/I 25.0 ND 95 60-140 <br /> Chiorobenzene 24.1 0.32 0.50 25.0 ND 96 60-140 <br /> 1,1-Dichloroethene 20.0 0.24 0.50 25.0 ND 8o 60-140 <br /> Toluene 25.4 0.32 0.50 25.0 ND 102 60-140 <br /> Trichloroethene 20.4 0.36 0.50 " 25.0 ND 82 60-140 <br /> Surrogate:Dibrwnofluoromethane 24.6 25.0 98 70-130 <br /> Surrogate:1,2-DCA-d4 14.8 " 2S.0 99 70-130 <br /> Surrogate:Toluene-d8 26.8 2S.0 107 70-130 <br /> Surrogate:4-BFB 24.2 " 2S.0 97 70-130 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document Unlew otherwise stated results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 10 of 14 <br />