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Page 3 of 3 <br /> Spargero Analytical Laboratory Division <br /> Mobile Laboratory Division <br /> Technok4yInc. Scientific Division <br /> With Automation in Mind <br /> EPA Method 8260 GCMS Analysis Report <br /> Method Blank <br /> Attention: Mr. Steve Giacomini Date Sampled: Apr 1, 1999 <br /> EMCON Date Received: Apr 2, 1999 <br /> 1433 North Market Blvd Date Analyzed: Apr 10, 1999 <br /> Sacramento, CA 95834 Invoice# 10967APR99 <br /> Project#: 16037-200.000 Project Name: Foothill Landfill <br /> Client ID: Method Blank LAB ID: 10967-MB <br /> Matrix: Water Dilution: 1: 1 <br /> Trace <br /> Name Concentration Concentration PQL MDL Units <br /> 56.) 1,3,5-trimethylbenzene ND 2.0 1.2 ug/I <br /> 57.) tert-butylbenzene ND 2.0 1.3 ug/I <br /> 58.) 1,2,4-trimethylbenzene ND 2.0 1.1 ug/I <br /> 59.) sec-butylbenzene ND 2.0 1.5 ug/I <br /> 60.) 1,3-dichlorobenzene ND 2.0 1.1 ug/I <br /> 61.) 1,4-dichlorobenzene ND 2.0 0.89 ug/I <br /> 62.) p-isopropyltoluene ND 2.0 1.2 ug/I <br /> 63.) 1,2-dichlorobenzene ND 2.0 0.95 ug/I <br /> 64.) n-butylbenzene ND 2.0 1.6 ug/I <br /> 65.) 1,2,-dibromo-3-chloropropane ND 2.0 1.2 ug/I <br /> 66.) 1,2,4-trichlorobenzene ND 2.0 1.1 ug/I <br /> 67.) Naphthalene ND 2.0 1.4 ug/I <br /> 68.) Hexachlorobutadiene ND 2.0 0.20 ug/I <br /> 69.) 1,2,3-trichlorobenzene ND 2.0 1.0 ug/I <br /> 70.) trans-1,4-dichloro-2-butene ND 2.0 1.3 ug/I <br /> Surrogate% Recovery of 1,2-dichloroethane-d4 = 94% <br /> Surrogate% Recovery of toluene-d8 = 108% <br /> Surrogate % Recovery of 4-Bromofluorobenzene= 109% <br /> ppb=parts per billion=ug/I=micrograms per liter <br /> ppm=parts per million=ug/ml=micrograms per milliliter <br /> ND=Not Detected. Compound(s)may be present at concentrations below the reporting limit. <br /> *=Trace Detected <br /> Apr 10, 1999 <br /> R.L.James,Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> 8260MBW.xls <br /> 3050 Fite Circle, Suite 112 9 Sacramento, California 95827 0 (996) 362-8947 • FAX(916) 362-0947 <br />