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1 <br /> Spargero Analytical Laboratory Division <br /> Mobile Laboratory Division <br /> Technobg-yInc. Scientific Division <br /> With Automation in Mind <br /> EPA Method 8260 GCMS <br /> Matrix Spike (MS) and Matrix Duplicate Spike (MSD) <br /> ' Attention: Mr. Steve Giacomini Date Sampled: Apr 1, 1999 <br /> EMCON Date Received: Apr 2, 1999 <br /> 1433 North Market Blvd Date Analyzed: Apr 10, 1999 <br /> Sacramento, CA 95834 Invoice#: 10967APR99 <br /> ' Project#: 16037-200.000 Project Name: Foothill Landfill <br /> Client ID: MS/MSD-Batch LAB ID: 10980-002MS <br /> 10980-002MSD <br /> Matrix: Water Dilution: 1: 1 <br /> UNITS= ug/l <br /> Sample Spike MS MSD QC Limits <br /> Compound Conc Added MS MSD % Rec % Rec RPD RPD % Rec <br /> 1,1-Dichloroethene ND 50 44 44 88% 88% 0% 20 61-145 <br /> Benzene ND 50 50 51 100% 102% 2% 20 76-127 <br /> Trichloroethene ND 50 47 48 94% 96% 2% 20 71-135 <br /> ' Toluene ND 50 45 46 90% 92% 2% 20 76-130 <br /> Ch lorobenzene ND50 40 41 80% 82% 2% 20 75-130 <br /> pp parts <br /> p billion <br /> -I ion ug/I micrograms per <br /> liter <br /> ppm=parts per million=ug/ml=micrograms per milliliter <br /> ND=Not Detected. Compound(s)may be present at concentrations below the detection limit. <br /> Apr 10, 1999 <br /> R. L.James,Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> 8260MSW.xIs <br /> 3050 Fite Circle, Suite 112 e Sacramento, California 95827 a (916) 362-8947 • FAX(916) 362-0947 <br />