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819 Striker Ave Ste 8 <br /> Sequoia Sacramento,CA 95834(916)921-960u <br /> Analytical FAX(916)92 t-C 100 <br /> J N%iva.se-4uoialabs.com <br /> Shaw E&I-Sacramento Project: Foothill Landfill,San Joaquin County 5308278 <br /> 1326 N.Market Blvd. Project Number: 791289/00003000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 08127/03 17:28 <br /> -- Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result %tDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3080260-EPA 5030B [P/T] <br /> Blank(3080260-BLKI) Prepared:08/19/03 Analyzed:08/20/03 <br /> Trichlorofluoromethane ND 0.42 0.50 ug/l <br /> 1,2,3-Trichloropropane ND 0.55 1.0 " <br /> 1,2,4-Trimethylbenzene ND 0.18 0.50 " <br /> 1,3,5-Trimethylbenzene ND 0.28 0.50 " <br /> Vinyl chloride ND 0.16 0.50 <br /> Xylenes(total) ND 0.48 0.50 <br /> Surrogate:DibromoJluoromethane 25.8 25.0 103 70-130 <br /> Surrogate:l,2-DCA-d4 26.1 25.0 104 70-130 <br /> Surrogate:Toluene-d8 24.5 25.0 98 70-130 <br /> Surrogate:4-BFB 24.9 25.0 100 70-130 " <br /> Blank(3080260-BLK21 Prepared&Analyzed:08/22/03 <br /> 2-Butanone ND 0.14 0.50 ug/l <br /> 2-Chloroethylvinyl ether ND 0.22 0.50 " <br /> 2-Hexanone ND 0.26 0.50 " <br /> 4-Methyl-2-pentanone ND 0.17 0.50 " <br /> Acetone 1.80 0.52 2.0 " J <br /> Acetonitrile ND 2.4 5.0 <br /> Acrolein ND 0.70 5.0 " <br /> Acrylonitrile ND 0.26 2.0 " <br /> Allyl chloride ND 0.14 0.50 " <br /> Carbon disulfide ND 0.29 0.50 " <br /> Chloroprene ND 0.10 0.50 " <br /> cis-1,3-Dichloropropene ND 0.11 0.50 11 <br /> Freon 113 ND 0.25 0.50 <br /> Iodomethane ND 0.036 0.50 " <br /> Isobutanol ND 0.61 1.0 " <br /> m,p-Xylene ND 0.38 0.50 <br /> Methacrylonitrile ND 0.73 1.0 <br /> Methyl methacrylate ND 0.20 0.50 " <br /> o-Xylene ND 0.15 0.50 <br /> Propionitrile ND 2.7 5.0 <br /> -- trans-l,3-Dichloropropene ND 0.10 0.50 " <br /> trans-l,4-Dichloro-2-butene ND 0.42 0.50 <br /> k Vinyl acetate ND 0.94 2.0 <br /> i Benzene ND 0.28 0.50 <br /> Bromobenzene ND 0.39 0.50 " <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 19 of 25 <br />