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Columbia Analytical Services,Inc. Sample Acceptance Check Form Client: Shaw Environmental&Infrastructure,Inc. Work order: P0900887 Project: Foothill Landfill, San Joaquin County/124591 (Ground Water) Sample(s)received on: 04/02/08 Date opened: 04/02/08 by: SSTAPLES Note: This form is used for all samples received by CAS. The use ofthis form for custody seals is strictly meant to indicate presence/absence and not as an indication of compliance or nonconformity. Thermal preservation and pH will only be evaluated either at the request of the client and/or as required by the method/SOP. Yes No N/A 1 Were sample containers properly marked with client sample ID? O ❑ ❑ 2 Container(s) supplied by CAS? ❑ 0 3 Did sample containers arrive in good condition? 0 ❑ ❑ 4 Were chain-of-custody papers used and filled out? 0 ❑ ❑ 5 Did sample container labels and/or tags agree with custody papers? 0 ❑ ❑ 6 Was sample volume received adequate for analysis? 0 ❑ ❑ 7 Are samples within specified holding times? 0 ❑ ❑ 8 Was proper temperature(thermal preservation)of cooler at receipt adhered to? ❑ ❑ Cooler Temperature °C Blank Temperature 3 °C 9 Was a trip blank received? 0 ❑ ❑ Trip blank supplied by CAS: Serial# 032$ -TB 1 10 Were custody seals on outside of cooler/Box? ❑ 0 ❑ Location of seal(s)? Sealing Lid? ❑ ❑ 0 Were signature and date included? ❑ ❑ 0 Were seals intact? ❑ ❑ 0 Were custody seals on outside of sample container? ❑ 0 ❑ Location of seal(s)? Sealing Lid? ❑ ❑ 0 Were signature and(late included? ❑ ❑ 0 Were seals intact? ❑ ❑ 0 I 1 Do containers have appropriate preservation,according to method/SOP or Client specified information? 0 ❑ ❑ Is there a client indication that the submitted samples are pH preserved? 0 ❑ ❑ Were VOA vials checked for presence/absence of air bubbles? 0 ❑ ❑ Does the client/method/SOP require that the analyst check the sample pH and if necessary alter it? 0 ❑ ❑ 12 Tubes: Are the tubes capped and intact? ❑ ❑ 0 Do they contain moisture? ❑ ❑ 0 13 Badges: Are the badges properly capped and intact? ❑ ❑ Ox Are dual bed badges separated and individually capped and intact? ❑ ❑ 0 s(tr Snmple 1p iGh>s►1ueRgysrd... eetvei ( c�jq�fecl ' A dTeudslrateeeip�f:P#rse(latraEu 1JGS£K1111rtfrr pH :; pIi l? Presellcr�Attsenwj Cari�mr'nts P0800887-001.01 40m1 VOA HCL <2 A P0800887-001.02 40ml VOA HCL A P0800887-001.03 40ml VOA HCL A P0800887-001.04 500mL Plastic NP P0800887-001.0$ 1500niL Plastic NP P0800887-001.06 500ml-Plastic HNO3 <2 P0800887-001.07 I I000ml AG NP Explain any discrepancies:(include lab sample ID numbers): 1 500ml plastic provided for TDS analysis. I liter ambers received for 8141 analysis is client supplied. *Required pH:Phenols/COD/NH3/TOC/TOX/NO3 i-NO2/T'KN/T.PHOS,H2SO4(pH<2),,Metals,HNO3(pH<2);CN(NaOH or NaOH/Asc Acid)(pH>I2); Diss.Sulfide,NaOH(pH>t 2);T.Sulfide,NnOWZnAC(pH>12) RSK-MEEPP,HCL(pH<2);RSK-CO2,(pH 5-8);Sulfur(pH>4) P0800997 Shaw 8nvimmental&Infrastrucluiv,Inc._Poothill Landfill,San Joaglun County_124591(Ground Water)-Page 1 of 2 04/04/08 6:41 PM