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COLUMBIA ANALYTICAL SERVICES, INC. Certificate.No: 02115CA Renew Date: 12/31/2005 109:010 007 EPA 200.7 Cadmium 109.010 009 EPA 200.7 Chromium 09.010 010 EPA 200.7 Cobalt __.... 109.010 011 EPA 200.7 - _ Copper 109.010 012 EPA 200.7 Iron 109.010 013 EPA 200.7 Lead 109.010 015 EPA 200.7 Manganese 109,010 016 EPA 200.7 _ Molybdenum 109.010 017 EPA 200.7 Nickel 109.010 019 EPA 200.7 Selenium 109.010 021 EPA 200.7 Silver 109.010 023 EPA 200.7 Thallium 09.010 024 EPA 200.7 Tin._. r109.010 026 EPA 200.7 Vanadium 109.010 027 EPA 200.7 Zinc 109.020 001 EPA 200.8 Aluminum _.. 109.020 0.02 EPA 200.8 Antimony " 909.020 003 EPA 200.8 Arsenic 109.020 004 EPA 200.8 Barium 109.020 005 EPA 200.8 Beryllium 109.020 006 EPA 200.8 Cadmium _ 109.020 007 EPA 200.8 Chromium 109.020 008 EPA 200.8 Cobalt 109.020 009 EPA 200.8 Copper 109.020 010 EPA 200.8 Lead 109.020 011 EPA 200.8 Manganese 109.020 012 EPA 200.8 Molybdenum 09.020 013 EPA 200.8 Nickel 109.020 014 EPA 200.8 Selenium 109.020 015 EPA 200.6 Silver - - ----- 109.020 016 EPA 200.8 Thallium "- 109.020 017 EPA 200.8 Vanadium 109.020 018 EPA 200.8 Zinc 109.050 001 EPA 206.2 Arsenic 109.081 .001 EPA 213.2 Cadmium 109.190 001 EPA 245.1 Mercury 109.280 001 EPA 270.2 Selenium 109.811 001 SM3500-Cr D Chromium(VI) 110-Volatile Organic Chemistry of Wastewater 110.020 001 EPA 602 Benzene 110.020 006 EPA 602 Ethylbenzene 110.020 007 EPA 602 Toluene 110.040 001 EPA 624 Benzene 110.040 002 EPA 624 - Bromodichioromethane 110.040 003 EPA 624 Bromoform 110.040 004 EPA 624 _ Bromomethane 110.040 005 EPA 624 Carbon Tetrachloride 110.040 006 EPA 624 Chlorobenzene As of 12/07/2004,this list supersedes all previous lists for this certificate number. Customers:Please verify the current accreditation standing with the State. Page 2 of 10