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McCampbell Analytical, Inc. <br />4 <br />110 2nd Avenue South, #D7, Pacheco, CA 94553-5560 <br />Telephone :925-798-1620 Fax:925-798-1622 <br />Website: www.mccanipbell.com E-mail: main@mccampbell.com <br />Allied Waste Client Project ID: #1733; STP -D-2002 <br />Date Sampled: 02/12/04 <br />Date Received: 02/13/04 <br />1145 West Charter Way <br />Date Extracted: 02/13/04 <br />Client Contact: Brad Bonner <br />Stockton, CA 95206 <br />Client P.O.: <br />Date Analyzed: 02/13/04 <br />Diesel (CIO -C23), Oil (C18+) Rang Extractable Hydrocarbons as Diesel and Motor Oil with Silica Gel Clean -Up* <br />Extraction method: SW3550C Analytical methods: SW8015C Work Order. 0402184 <br />Lab ID <br />Client ID <br />Matrix <br />TPH(d) <br />TPH(mo)DF <br />% SS <br />0402184-UU I A <br />Comp #I S <br />2400,g,b <br />6500 <br />5 95 <br />------------- <br />— <br />– <br />i j <br />i <br />I <br />I <br />I <br />f <br />-- -- ----- <br />Reporting Limit for DF =1; <br />Reporting <br />W <br />NA NA <br />I ug/L <br />ND means not detected at or <br />-- <br />S <br />– ---- -- _ <br />1.0 5.0 <br />}— -- <br />mg/Kg <br />above the reporting limit <br />I <br />* water samples are reported in µg/L, wipe samples in pg/wipe, soil/solid/sludge samples in mg/kg, product/oil/non-aqueous liquid samples in mg/L, <br />and all DISTLC / STLC / SPLP / TCLP extracts are reported in µg/L. <br /># cluttered chromatogram resulting in coeluted surrogate and sample peaks, or; surrogate peak is on elevated baseline, or; surrogate has been diminished <br />by dilution of original extract. <br />+The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation: a) <br />unmodified or weakly modified diesel is significant; b) diesel range compounds are significant; no recognizable pattern; c) aged diesel? is significant); <br />d) gasoline range compounds are significant; e) unknown medium boiling point pattern that does not appear to be derived from diesel; f) one to a few <br />isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheen/product is present; i) liquid sample that contains <br />greater than –2 vol. % sediment; k) kerosene/kerosene range; l) bunker oil; m) fuel oil; n) stoddard solvent/mineral spirit. <br />DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />