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0 <br />0 <br />C <br />U <br />D <br />Laboratory Control Spike Recoveries <br />EPA 8260B <br />APPL ID: 07101OW-68295 LCS -116935 <br />Batch ID: $82C2-071009AC <br />APPL Inc. <br />4203 West Swift Avenue <br />Fresno, CA 93722 <br />Compound Name <br />Spike Lvl <br />SPK Result <br />DUP Result <br />SPK % <br />DUP % <br />Recovery <br />RPD <br />RPD <br />Analysis Date : <br />ug/L <br />ug/L <br />ug/L <br />Recovery <br />Recovery <br />Limits <br />% <br />Limits <br />1,1,1,2 -Tetrachloroethane <br />10.00 <br />9.96 <br />10.3 <br />99.6 <br />103 <br />70-130 <br />3.4 <br />20 <br />1,1,1 -Trichloroethane <br />10.00 <br />8.93 <br />9.41 <br />89.3 <br />94.1 <br />70-130 <br />5.2 <br />20 <br />1,1,2,2 -Tetrachloroethane <br />10.00 <br />9.53 <br />10.1 <br />95.3 <br />101 <br />70-130 <br />5.8 <br />20 <br />1,1,2 -Trichloroethane <br />10.00 <br />9.04 <br />9.12 <br />90.4 <br />91.2 <br />70-130 <br />0.88 <br />20 <br />1,1-Dichloroethane <br />10.00 <br />9.04 <br />9.45 <br />90.4 <br />94.5 <br />70-130 <br />4.4 <br />20 <br />1,1-Dichloroethene <br />10.00 <br />9.03 <br />9.67 <br />90.3 <br />96.7 <br />70-130 <br />6.8 <br />20 <br />1,2,3-Trichloropropane <br />10.00 <br />9.57 <br />10.0 <br />95.7 <br />100 <br />70-130 <br />4.4 <br />20 <br />1,2,4-Trichlo robe nzene <br />10.00 <br />9.17 <br />10.1 <br />91.7 <br />101 <br />70-130 <br />9.7 <br />20 <br />1,2-Dibromo-3-chloropropane <br />10.00 <br />9.06 <br />9.61 <br />90.6 <br />96.1 <br />70-130 <br />5.9 <br />20 <br />1,2-Dibromoethane <br />10.00 <br />9.80 <br />10.4 <br />98.0 <br />104 <br />70-130 <br />5.9 <br />20, <br />1,2 -Dichlorobenzene <br />10.00 <br />9.64 <br />10.2 <br />96.4 <br />102 <br />70-130 <br />5.6 <br />20 <br />1,2-Dichloroethane <br />10.00 <br />8.79 <br />9.03 <br />87.9 <br />90.3 <br />70-130 <br />2.7 <br />20 <br />1,2-Dichloroethene-(cis) <br />10.00 <br />8.95 <br />9.31 <br />89.5 <br />93.1 <br />70-130 <br />3.9 <br />20 <br />1,2-Dichloroethene-(trans) <br />10.00 <br />8.61 <br />9.24 <br />86.1 <br />92.4 <br />70-130 <br />7.1 <br />20 <br />1,2-Dichloropropane <br />10.00 <br />9.08 <br />9.23 <br />90.8 <br />92.3 <br />70-130 <br />1.6 <br />20 <br />1,3 -Dichlorobenzene <br />10.00 <br />9.69 <br />10.1 <br />96.9 <br />101 <br />70-130 <br />4.1 <br />20 <br />1,3-Dichloropropene-(cis) <br />10.00 <br />8.75 <br />8.98 <br />87.5 <br />89.8 <br />70-130 <br />2.6 <br />20 <br />1,3-Dichloropropene-(trans) <br />10.00 <br />8.96 <br />9.08 <br />89.6 <br />90.8 <br />70-130 <br />1.3 <br />20 <br />1,4 -Dichlorobenzene <br />10.00 <br />9.70 <br />10.2 <br />97.0 <br />102 <br />70-130 <br />5.0 <br />20 <br />2-Butanone <br />10.00 <br />9.24 <br />9.05 <br />92.4 <br />90.5 <br />70-130 <br />2.1 <br />20 <br />2-Hexanone <br />10.00 <br />10.5 <br />10.1 <br />105 <br />101 <br />56-136 <br />3.9 <br />20 <br />4-Methyl-2-pentanone <br />10.00 <br />9.67 <br />10.0 <br />96.7 <br />100 <br />70-130 <br />3.4 <br />20 <br />Acetone <br />10.00 <br />9.50 <br />9.66 <br />95.0 <br />96.6 <br />26-181 <br />1.7 <br />20 <br />Acrylonitrile <br />10.00 <br />9.08 <br />8.97 <br />90.8 <br />89.7 <br />70-130 <br />1.2 <br />20 <br /># = Recovery is outside QC limits. <br />Comments: <br />11 <br />Primary <br />SPK <br />DUP <br />Quant Method : <br />C82C2.M <br />C82C2.M <br />Extraction Date : <br />10/10/2007 <br />10/10/2007 <br />Analysis Date : <br />10/10/2007 <br />10/10/2007 <br />Instrument : <br />Chico <br />Chico <br />Run: <br />1009C14 <br />1009C15 <br />Initials : <br />ND <br />Printed: 10/17/2007 11:50:58 AM <br />APPL Standard LCSD <br />