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1 <br />1 <br />1 <br />7 <br />1 <br />1 <br />1 <br />1 <br />t <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />Laboratory Control Spike Recoveries <br />EPA 8260B <br />APPL ID: 07101OW-68295 LCS -116935 <br />Batch ID: $82C2-071009AC <br />SPK <br />DUP <br />Quant Method : <br />APPL Inc. <br />4203 West Swift Avenue <br />Fresno, CA 93722 <br />C82C2.M <br />Compound Name <br />Spike Lvl <br />SPK Result <br />DUP Result <br />SPK % <br />DUP % <br />Recovery <br />RPD <br />RPD <br />Run: <br />ug/L <br />ug/L <br />ug/L <br />Recovery <br />Recovery <br />Limits <br />% <br />Limits <br />Tetrachloroethene <br />10.00 <br />9.71 <br />10.5 <br />97.1 <br />105 <br />70-130 <br />7.8 <br />20 <br />Toluene <br />10.00 <br />8.85 <br />9.10 <br />88.5 <br />91.0 <br />70-130 <br />2.8 <br />20 <br />trans-1,4-Dichloro-2-butene <br />10.00 <br />9.32 <br />9.79 <br />93.2 <br />97.9 <br />70-130 <br />4.9 <br />20 <br />Trichloroethene <br />10.00 <br />9.17 <br />9.48 <br />91.7 <br />94.8 <br />70-130 <br />3.3 <br />20 <br />Trichlorofluoromethane <br />10.00 <br />9.27 <br />9.95 <br />92.7 <br />99.5 <br />70-131 <br />7.1 <br />20 <br />Vinyl Acetate <br />10.00 <br />9.67 <br />9.85 <br />96.7 <br />98.5 <br />70-130 <br />1.8 <br />20 <br />Vinyl chloride <br />10.00 <br />9.44 <br />9.49 <br />94.4 <br />94.9 <br />70-141 <br />0.53 <br />20 <br />Xylenes <br />----------------- <br />30.0 <br />29.9 <br />30.9 <br />99.7 <br />103 <br />70-130 <br />3.3 <br />20 <br />---------------------------------------------------------------------------------------------------------------------------------------------------------------- <br />Surrogate: 1,2-Dichloroethane-d4 <br />18.5 <br />- <br />18.8 <br />18.6 <br />- <br />102 <br />101 <br />70-130 <br />Surrogate:4-Bromofluorobenzene <br />22.1 <br />22.5 <br />22.3 <br />102 <br />101 <br />70-130 <br />Surrogate: Dibromofluoromethane <br />18.7 <br />18.8 <br />18.7 <br />100 <br />99.9 <br />70-130 <br />Surrogate: Toluene -d8 <br />-------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- <br />22.4 <br />22.6 <br />22.3 <br />101 <br />99.5 <br />70-130 <br /># = Recovery is outside QC limits. <br />Comments: <br />13 <br />Primary <br />SPK <br />DUP <br />Quant Method : <br />C82C2.M <br />C82C2.M <br />Extraction Date : <br />10/10/2007 <br />10/10/2007 <br />Analysis Date : <br />10/10/2007 <br />10/10/2007 <br />Instrument : <br />Chico <br />Chico <br />Run: <br />1009C14 <br />1009C15 <br />Initials : <br />ND <br />Printed: 10/17/2007 11:50:58 AM <br />APPL Standard LCSD <br />