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LABORATORIES, INC. Herst Associates Project: NCYC Reported: 03/03/2008 14:50 4630 South Highway 94 North Outer Road Project Number: [none] Saint Charles,MO 63304 Project Manager: David Vasbinder Volatile Organic Analysis (EPA Method8260) BCL Sample ID: 0802520-09 Client Sample Name: Trip Blank,2/2212008 12:00:00AM Prep Run Instru- QC MB Lab Constituent Result Units PQL IIOIDL Method Date Date/Time Analyst ment lD Dilution Batch lD Blas Quals t-Butyl alcohol NO ug1L 10 8.6 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 NO - _.. _..............._. __........_........- --__._..........--...... — Carbon disulfide ND ug/L 1.0 0.40 EPA-8260 02/27/08 02/28/08 23:14 MGC MS V5 1 BRB1714 ND -------—. - ----...._..... —..........-- ..._.. ..._._.............__ trans-1,4-Dichioro-2-butene ND ug/L 5.0 2.0 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 NO _.- ..__........--.._. -------._.... Diisopropyl ether ND ug/L 0.50 0.18 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 ND ._.------ ........... - . .....__.— _..__..._...__ ....-__...__—_._..........- -----__ ........_... - - --- ........._------- ...................-._.. _ Ethanol ND ug/L 250 57 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 ND -._.—._.._.-...........---.._.........-.............- -.......---............... _ ...... ..._.._....._...._.__—.-...._...._...............--...-- -- - _ - ----- -- Ethyl t-butyl ether ND ug/L 0.50 0.22 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 9 BRB1714... NO -- --......_....... ------ - -.......... 2-Hexanone NO ug/L 10 2.5 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 ND _..__............. ................-.__._._....._.._..._—.--......--------- _......__....-..._................. .-- -.........._...... - - -..—._.._._- _ Methyl ethyl ketone ND ug/L 10 1.6 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 NO -_-- - _ _ - ._._... ..................._ _ .............-...--- ----------- --__.......................... Methyl Iodide ND ug/L 2.0 0.42 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1_._.._._. BRB1714. ND ..-_ _._ ------ --._.-.......... -- ----- -— ............._ .. _ —....__. Methyl isobutyl ketone ND ugiL 10 3.4 EPA-8260 02/27/08 02128/08 23:14 MGC MS-V5 1 BRB1714 ND _............_... Vinyl acetate ND ug/L 10 3.1 EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 ND -- ---.....__........-......-_- 1,2-Dichloroethane-d4(Surrogate) 104 % 76-114 (LCL-UCL) EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 _.—.--- ._............._.-._._..__ _—_ —._.._._.._....-- ...... -------..........._........... Toluene-d8(Surrogate) 101 % 88-110 (LCL-UCL) EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 .......-------------------------_............. - 4-Bromofluorobenzene(Surrogate) 101 % 86-115 (LCL-UCL) EPA-8260 02/27/08 02/28/08 23:14 MGC MS-V5 1 BRB1714 BC Laboratories The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party.BC Laboratories,Inc.assumes no responsibility for report alteration,separation, detachment or third party interpretation. Pagc 29 of 35 4100 Atlas Court-Bakersfield,CA 93308-(661)327-4911 -FAX(661)327-1918-www.bclabs.com ® M ® M ® M ® ® ® ® ® M = ® M