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is, two consecutive sets of similar field measurements will be ob- <br /> tained. Purged water is stabilized when (1) the pH is within ±0.1 pH <br /> units, (2) specific conductance is within ±5 percent, or (3) tempera- <br /> ture is within ±1 .0°F. All records of the above data will be kept on <br /> a field data sheet. Figure A-1 shows an example of the Water Sample <br /> Field Data Sheet. Copies of the field data sheets will be subjected <br /> to review by the sampling supervisor upon completion of the sampling <br /> event. The pH, specific conductance, and temperature meter will be <br /> calibrated daily prior to initiating field activities. The calibra- <br /> tion will be checked once each day to verify meter performance. <br /> Sampling Procedures <br /> Samples will be collected after the calculated purge volume has been <br /> removed and the pH, conductance, and temperature have stabilized. <br /> With as little interruption in pumping rates as possible, the bladder <br /> pump effluent will be directed into appropriate containers. The pump <br /> flow will be regulated when collecting samples for volatile organic <br /> analysis. The flow will be set to approximately 100 milliliters per <br /> minute to minimize turbulence and aeration of the pump effluent. <br /> Sample bottles for volatile organics analysis will be filled complete- <br /> ly to prevent any air from remaining in the bottle. A positive menis- <br /> cus forms when the bottle is completely full . A convex, Teflon-lined <br /> septum will be placed over the positive meniscus to seal the contain- <br /> er. After capping, the bottle will be inverted and tapped to check <br /> that no air bubbles are present. <br /> All samples will be collected in duplicate. The sample containers for <br /> other parameters will be filled, preserved as required, and capped. <br /> Samples for metals analysis will be filtered in the field prior to <br /> preservation with nitric acid. Filters will be discarded after each <br /> use. <br /> PJ9 9390207.00D A-3 <br />