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April 4, 2012 Lab ID : STK1232392 <br /> San Joaquin County Solid Waste Customer : 3-2956 <br /> Quality Control - Organic <br /> Constituent Method Date/ID Type Units Conc. QC Data DQO Note <br /> Organic <br /> 1,1,1,2-Tetrachloroethane 5030B 03/23/12:203289VRG Blank u /L ND <0.5 <br /> 1,1,1-Trichloroethane(TCA) 5030B 03/23/12:203289VRG Blank ugLL ND <0.5 <br /> 1,1,2,2-Tetrachloroethane 5030B 03123/12:203289VRG Blank ugfl, ND <0.5 <br /> 1,1,2-Trichloroethane 5030B 03/23/12:203289VRG Blank ugIL ND <0.5 <br /> 1,1,2-Trichlorotrifluoroethane 5030B 03/23/12:203289VRG Blank ug/L ND <1 <br /> 1,1-Dichloroethane 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,1-Dichloroethylene 5030B 03/23/12:203289VRG Blank ug/L. ND <0.5 <br /> LCs ug/L 25.00 98.3% 22-204 <br /> MS ug/L 25.00 121% 22-204 <br /> (STK1232302-003) MSD ug/L 25.00 117% 22-204 <br /> MSRPD I u 25.00 1 3.3% :526.9 <br /> 1,1-Dichloro ro ene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,2,3-Trichlorobenzene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,2,3-Trichlororo ane 5030B 03/23/12:203289VRG Blank ugIL ND <1 <br /> 1,2,4-Trichlorobenzene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,2,4-Trimeth lbenzene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,2-Dibromoethane(EDB) 5030B 03123/12:203289VRG Blank u ND <2 <br /> 1,2-Dichlorobenzene 5030E 03/23112:203289VRG Blank u ND <0.5 <br /> 1,2-Dichloroethane(EDC) 5030B 03/23/12:203289VRG Blank I ugND <0.5 <br /> 1,2-Dichloroethane-d4 5030B 03/23/12:203289VRG Blank ug/L 25.00 110% 73-138 <br /> LCS ug/L 25.00 ill% 73-138 <br /> MS ug/L 25.00 113% 73-163 <br /> (STK1232302-003) MSD ug/L. 25.00 112% 73-163 <br /> MSRPD u 25.00 0.9% 520.0 <br /> 1,2-Dichloro ro ane 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,3,5-Trimeth lbenzene 5030B 03/23112:203289VRG Blank I u ND 1 <0.5 <br /> 1,3-Dichlorobenzene 5030B 03123/12:203289VRG Blank u ND <0.5 <br /> 1,3-Dichloro ro ane 5030B 03/23112:203289VRG Blank ug/L ND <0.5 <br /> 1,4-Dichlorobenzene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 1,4-Dioxane 5030B 03/23112:203289VRG Blank u ND <200 <br /> 2-Dichloro ro ane 5030B 03/23/12:203289VRG Blank uEL ND <0.5 <br /> Butanone K 5030B 03/23/12:203289VRG Blank u ND <10 <br /> -Chloroeth lvin 1 ether 5030B 03123/12:203289VRG Blank u ND <10 <br /> 2-Chlorotoluene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> 2-Hexanone 5030B 03/23/12:203289VRG Blank u ND <10 <br /> Bromofluorobenzene 5030B 03/23/12:203289VRG Blank ug/L 25.00 102% 80-127 <br /> LCs ug/L 25.00 99.3% 80-127 <br /> MS ug/L 25.00 101% 88-114 <br /> (STK1232302-003) MSD ug/L 25.00 101% 88-114 <br /> MSRPD I ug/L 25.00 0.07% :520.0 <br /> Chlorotoluene 5030B 03/23/12:203289VRG Blank ugND <0.5 <br /> Meth 1-2- entanone(MIBK) 5030B 63/23/12:203289VRG Blank u ND <10 <br /> Acetone 5030B 03/23/12203289VRG Blank ugND <10 <br /> Acetonitrile 5030B 03/23/12:203289VRG Blank u ND <50 <br /> Acrolein 5030B 03/23/12:203289VRG Blank ug/L ND <50 <br /> Amy <br /> lonitrile 5030B 03/23/12:203289VRG Blank u ND <50 <br /> All I Chloride 5030B 03/23/12:203289VRG Blank ug/L ND <10 <br /> Benzene 5030B 03123/12:203289VRG Blank ug/L ND <0.5 <br /> LCS ug/L 25.00 99.1% 61-127 <br /> MS ug/L 25.00 112% 61-127 <br /> (STK1232302-003) MSD ug/L 25.00 109% 61-127 <br /> MSRPD u 25.00 2.1% _:17.5 <br /> Bromobenzene 5030B 03/23/12:203289VRG Blank u ND <0.5 <br /> ® romochloromethane 5030B 03/23/12:203289VRG Blank u ND <1 <br /> romodichloromethane I 5030B 03/23/12:203289VRG I Blank I u ND 1 0.5 <br />