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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Results <br /> Client: Shaw Environmental&Infrastructure,Inc Service Request: P0700376 <br /> Project: Corral Hollow Landfill,San Joaquin County/124592(Ground Water) Date Collected: 04/16/2007 <br /> Sample Matrix: Water Date Received: 04/17/2007 <br /> Volatile Organic Compounds <br /> Sample Name: SB-1 Units: ug/L <br /> Lab Code: P0700376-003 Basis: NA <br /> Extraction Method: EPA 5030B Level: Low <br /> Analysis Method: 82608 <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> Vinyl Chloride ND U 0.50 0.43 1 04/18/07 04/18/07 PWG0700595 <br /> Control Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> Dibromofluoromethane 102 73-129 04/18/07 Acceptable <br /> Toluene-d8 92 76-122 04/18/07 Acceptable <br /> 4-Bromofluorobenzene 86 63-118 04/18/07 Acceptable <br /> Comments: <br /> 13 <br /> Printed: 04/25/2007 10:50:27 Form I-Organic Page 3 of 3 <br /> P:\STEALTMCRYSTAL.RPT%Fonnlm.apt Merged Superset Reference: RR13545 <br />