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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Results <br /> Client: Shaw Environmental&Infrastructure,Inc Service Request: P0600138 <br /> Project: Harney Lane Landfill,San Joaquin County/791290/0004000 Date Collected: 10/18/2006 <br /> Sample Matrix: Water Date Received: 10/19/2006 <br /> Volatile Organic Compounds <br /> Sample Name: MW-3 <br /> Lab Code: P0600138-003 Units: ug/L <br /> Basis: NA <br /> Extraction Method: METHOD Level: Low <br /> Analysis Method: 624M <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> Trichlorofluoromethane ND U 1.0 0.60 1 10/28/06 10/28/06 PWG0601542 <br /> Vinyl Chloride ND U 0.50 0.43 1 10/28/06 10/28/06 PWG0601542 <br /> Control Date <br /> Surrogate Name %Ree Limits Analyzed Note <br /> 1,2-Dichloroethane-d4 93 75-124 10/28/06 Acceptable <br /> 4-Bromofluorobenzene 86 69-120 10/28/06 Acceptable <br /> Toluene-d8 95 84-115 10/28/06 Acceptable <br /> Analyte Comments <br /> 1,1,2-Trichlorotrifluoroethane This analyte is not listed in EPA Method 624 <br /> cis-l,2-Dichloroethene This analyte is not listed in EPA Method 624 <br /> Dichlorodifluoromethane This analyte isnot listed in EPA Method 624 <br /> Total Xylenes This analyte is not listed in EPA Method 624 <br /> Methyl tert-Butyl Ether This analyte is not listed in EPA Method 624 <br /> Comments: <br /> Printed: 10/31/2006 09:15:52 Form 1 A-Organic <br /> PASTEALMCRYSTAL.RPT1Form1m.rpt Merged Page 2 of 2 <br /> Superset Reference: 1ZR13177 <br />