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COLUMBIA ANALYTICAL.SERVICES,INC. <br /> Analytical Results <br /> Client: Shaw Environmental&Infrastructure,Inc Service Request: P0600138 <br /> Protect: Harney Lane Landfill,San Joaquin County/791290/0004000 Date Collected: NA <br /> Sample Matrix: Water Date Received' NA <br /> 1 <br /> Sample Name: Method Blank Volatile Organic Compounds <br /> Units: ug/L <br /> Lab Code: PWG0601542-3 Basis: NA <br /> Extraction Method: METHOD Level: Low <br /> Analysis Method: 624M <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> Trichlorofluoromethane ND U 1.0 0.60 1 10/28/06 10/28/06 PWG0601542 <br /> Vinyl Chloride ND U 0.50 0.43 1 10/28/06 10/28/06 PWG0601542 <br /> ate Name o Control Date <br /> Surrogate /oRec Limits Analyzed Note <br /> 1,2-Dichloroethane-d4 96 75-124 10/28/06 Acceptable <br /> 4-Bromofluorobenzene 89 69-120 10/28/06 Acceptable <br /> Toluene-d8 96 84-115 10/28/06 Acceptable <br /> 1 <br /> t Analyte Comments <br /> 1,1,2-Trichlorotrifluoroethane This analyte is not listed in EPA Method 624 <br /> cis-1,2-Dichloroethene This analyte is not listed in EPA Method 624 <br /> Dichlorodifluoromethane This analyte is not listed in EPA Method 624 <br /> Total Xylenes This analyte is not listed in EPA Method 624 <br /> ' Methyl tert-Butyl Ether This analyte is not listed in EPA Method 624 <br /> Comments: <br /> 18 <br /> Printed: 10/31/2006 09:15:58 Form I-Organic <br /> P:\STEAL'rMCRYSTAL.RPTIFonnlm.rpt Merged Page 2 of 2 <br /> Superset Reference: RR13177 <br />