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COLUMBIA ANALYTICAL SERVICES,INC. Certificate No: 1296 <br /> Renew Date: 07/31/2006 <br /> 116.040 041 Methyl tert-butyl Ether(MTBE) EPA 80216 _ <br /> 116.040 062 BTEX EPA 8021 B <br /> 116.080 000 Volatile Organic Compounds EPA 8260B <br /> 116.080 120 Oxygenates EPA 8260B — <br /> 116.100 001 Total Petroleum Hydrocarbons-Gasoline LUFT GC/MS <br /> 116.100 010 BTEX and MTBE LUFT GC/MS <br /> 116.110 001 Total Petroleum Hydrocarbons-Gasoline LUFT <br /> Field of Testing: 117-Semi-volatile Organic Chemistry of Hazardous Waste <br /> 117.010 001 Diesel-range Total Petroleum Hydrocarbons EPA 8015B <br /> 117.016 001 Diesel-range Total Petroleum Hydrocarbons LUFT <br /> - - ------- - <br /> 117.110 000 Extractable Organics EPA 8270C <br /> 117.210 000 Organochlorine Pesticides EPA 8081A <br /> 117.220 000 PCBs EPA 8082 <br /> As of 08/30/2005,this list supersedes all previous lists for this certificate number. <br /> Customers: Please verify the current accreditation standing with the State. Page 3 of <br />