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COLUMBIA ANALYTICAL SERVICES,INC. Certificate rtiflcate No: 02115CA Renew Date: 12/31/2005 111.170 015 EPA 608 Endrin Aldehyde - 111.170 016 EPA 608 Heptachlor 111.170 017 EPA 608 Heptachlor Epoxide 111.170 018 EPA 608 _ Toxaphene 111.170 019 EPA 608 PCB-1016 - 111.170 020 EPA 608 _ PCB-1221 111.170 021 EPA 608 PCB-1232 111.170 022 EPA 608 PCB-1242 ----- -- 11 1.170 023 EPA 608 PCB-1248 111.170 024 EPA 608 PCB 1254 111.170 025 EPA 608 PCB-1260 111.271 001 EPA 1664 Oil and Grease 114-Inorganic Chemistry of Hazardous Waste 114.010 001 EPA 6010B Antimony 14.010 002 EPA 6010B Arsenic 114.010 003 EPA 6010B Barium _ 114.010 004 EPA 60108 Beryllium 114.010 005 EPA 6010B Cadmium 114.010 006 EPA 6010B Chromium 114.010 007 EPA 6010B Cobalt 114.010 008 EPA 6010B Copper 114.010 009 EPA-601-0-B----.. Lead -- --- ---- 114.010 010 EPA 60106 Molybdenum 114.010 011 EPA 6010B Nickel 114.010 012 EPA 6010B Selenium 114.010 013 EPA 6010B Silver 114.010 015 EPA 60108 Vanadium 114.010 016 EPA 6010B Zinc 114.020 001 EPA 6020 Antimony 114.020 002 EPA 6020 Arsenic 114.020 003 EPA 6020 Barium 114.020 004 EPA 6020 Beryllium 114.020 005 EPA 6020 Cadmium 114.020 006 EPA 6020 Chromium 114.020 007 EPA 6020 Cobalt 114.020 008 EPA 6020 Copper 114.020 009 EPA 6020 Lead 114.020 010 EPA 6020 Molybdenum 114.020 011 EPA 6020 Nickel ------------ -- _-------- 114.020 012 012 EPA 6020 - ---- - - - Selenium 114.020 013 EPA 6020 Silver 114.020 014 EPA 6020 Thallium 114.020 015 EPA 6020 Vanadium 114.020 016 EPA 6020 Zinc 114.040 001 EPA 7060A Arsenic 114.103 001 EPA 7196A Chromium(VI) 114.131 001 EPA 7421 Lead 114.140 001 EPA 7470A Mercury As of 12/07/2004,this list supersedes all previous lists for this certificate number. Customers:Please verify the current accreditation standing with the State. Page 5 of 10