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COLUMBIA ANALYTICAL SERVICES,INC. <br /> QA/QC Report <br /> Client: Shaw Environmental&Infrastructure,Inc. Service Request: P0700023 <br /> Project Name: Harney Lane Landfill,San Joaquin County Date Collected: 01/10/07 <br /> Project Number: 791290(Ground Water) Date Received: 01/11/07 <br /> Sample Matrix : WATER Date Extracted: NA <br /> Date Analyzed : 01/11/07 <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> Sample Name : MW3 Units: mg/L(ppm) <br /> Lab Code: P0700023-003MS P0700023-003DMS Basis: NA <br /> Test Notes: <br /> Spike <br /> Prep Analysis Spike Level Sample Spike Result Recovery CAS Relative <br /> Acceptance Percent Result <br /> Analyte Method Method <br /> PQL MS DMS Result MS DMS MS DMS Limits Difference Notes <br /> Chloride None 300.0 0.5, 10.0 10.0 13.6 23.5 23.5 99 99 80-120 <1 <br /> 1 <br /> Approved B i' , <br /> PP y ( ( <br /> Date <br /> Report By:RWONG <br />