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APPENDIX D <br /> SAMPLING AND ANALYSIS PLAN <br /> The sampling and analysis procedures for the compost leachate monitoring program at the Tracy <br /> Materials Recovery & Transfer Facility are presented in this appendix. The procedures will <br /> provide for consistent and reproducible sampling methods; proper application of analytical <br /> methods; accurate and precise analytical results; and provide guidelines so that the overall <br /> objectives of the monitoring program are achieved. <br /> The following documents have been used as guidelines for the development of these procedures: <br /> 0 <br /> Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater, <br /> EPA-600/4-82-057, July 1982 <br /> • Met for Chemical Analysis of Water and Wastes, EPA-600/4-79-020,revised <br /> March 1983 <br /> • RCRA Groundwater Monitoring Technical Enforcement Guidance Document, <br /> OS 9950.1, September 1986 <br /> • Test Methods for Evaluating Solid Waste: Physical/Chemical Methods, EPA SW- <br /> 846, 3rd edition, November 1986 <br /> SAMPLE COLLECTION <br /> Sample collection procedures include equipment cleaning and compost leachate sampling. <br /> Equipment Cleaning <br /> Sample bottles, caps, and septa used in sampling for volatile and sernivolatile organics shall be <br /> triple rinsed with high-purity deionized water. After being rinsed, sample bottles shall be dried <br /> overnight at 200°C. Sample caps and septa shall be dried overnight at 60°C. Sample bottles, <br /> caps, and septa shall be protected from solvent contact between drying and actual use at the <br /> sampling site. Sample bottles, caps, and septa shall be used only once and discarded after <br /> analysis is complete. <br /> LAPR0JECT\397\MRMC14.TCY D-1 Fekuwy 1,1996 <br />