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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> I24 http//wwwmcc@mRbellco E-mail main@mccampbell corn <br /> i <br /> IAdvanced GeoEnvironmental Client Project ID Waterloo Food&Fuel Date Sampled 01/05/01 <br /> 4005 North Wilson Way Date Received 01/09/01 <br /> Stockton, CA 95205 Client Contact Bili Little Date Extracted 01/12/01 <br /> Client P O Date Analyzed 01/12/01 <br /> I7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 57427 57428 57429 57430 <br /> MW1/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client ID 010501 010501 010501 010501 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIKE) ND<125 ND<5000 ND<2500 ND<5000 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND<125 ND<5000 ND<2500 ND<5000 50 10 <br /> Methyl-tert Butyl Ether(MTBFs) 6500 310,000 140,000 280,000 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<125 ND<5000 ND<2500 ND<5000 50 10 <br />' text-Butanol ND<625 ND<25,000 ND<12500 ND<25,000 25 50 <br />' Methanol ND<25,000 ND<1000,000 ND<500,000 ND<1000,000 1000 200 <br />' Ethanol ND<6250 ND<250,000 ND<125,000 ND<250,000 250 50 <br /> Surrogate Recoveries(%) <br /> Dtbromotluoromcthane 110 109 108 107 <br />' Comments <br />' *water samples are reported to ug/L,soil and sludge samples to ug/kg,wipes to ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(t)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br />' high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />