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f <br /> 110 Second Avenue Saute;,#07,Pacheco CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 9Z5-798-1620 Fax 925-798-1622 <br /> httP//www mccam bell cum E-mail rnam@rriccampbell com <br /> Advanced GeoEnvuroiimental Client Project ID Waterloo Food And Date Sampled 021l 6199 <br /> 4005 North Wilson Way Fuel Date Received 02/17/99 <br /> Stockton,CA 95205 Client Contact Bob Marty Date Extracted 02/17/99 <br /> Client P O Date Analyzed 02/17199 <br /> EPA analytical method&WI O/290 7,239 2' Lead* <br /> Lith 1D Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 03590 SP-6 S TLC 10 95 <br /> 03581 SP-7 S TTLC 71 97 <br /> 03582 SS-1-T6N S TTLC 95 95 <br /> 03583 SS-2-T5N S 'TTLC 915 94 <br /> 03584 SS-3-T5S S TTLC 79 97 <br /> 03585 SS-4-T6S S TTLC 79 93 <br /> S TTLC 3 0 mB&8 <br /> Reporting Urmt unless otherwiae <br /> stated,ND means not detected above W TTLC 0 005 ritg/L <br /> the repotting linut <br /> STLC TCLP 0 2 mg/L <br /> 'soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water aamples and all STLC 1 SPLP 1 TCI,P extracts in me/I. <br /> `Lead i3 analysed using bPA method 6D]0 (ICP)fvr=13 sludges STLC& TCLP extracts and method 239 2 (AA t-uriiace) for water <br /> sarrtples <br /> 'EPA exbaction metitoda 1311(TCI P) 3010/3020(wator,TTLC) 3040(oigan)c maericts.TTLC),3050(solnde TTLC) STLC-CA Title 22 <br /> `surrogate dilutird out of range,N/A trims surrogate not appltcahte tv this analysis <br /> a reporting limit raised due imtnx mierfrnnee <br /> i) liquid sample that contains greater than —2 vat % sadtrncnt this sedirmnt is extracted +nil+ the liquid, in accoidancc with EPA <br /> rrnethodolognee and can aignillcandy effect reported metal concentrations <br /> DHS Ceftfitcadon No 1644 �,�Edward Haiuiilton,Lab Directox <br />