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1102nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> J4 h9p//www mccampbell corn E-mail main@mccampbell corn <br /> • <br /> Advanced GeoEnvironmental Client Project ID Waterloo Food&Fuel Date Sampled 01/25 & 01/26/00 <br /> 4005 North Wilson Way Date Received 01/28/00 <br /> 1 Stockton, CA 95205 Client Contact Tony Mtkacich Date Extracted 01/28/00 <br />' Client P O Date Analyzed 01/28-01/31/00 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 29795 29799 29801 29803 <br /> Reporting Lima <br /> Client ID MW-3-15' MW-3-35' MW-3-45' MW-3-55' <br />' Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(D1PE) ND ND<100 ND<200 ND<500 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND<100 ND<200 ND<500 50 10 <br /> Methyl-tert Butyl Ether{MTBE) ND 2700 7800 20,000 50 to <br /> lie <br /> tent-Amyl Methyl Ether(TAME) ND ND<100 ND<200 ND<500 50 1 0 <br /> tert-Butanol ND ND<500 ND<1000 ND<2500 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 104 107 90 91 <br /> Comments <br /> *water samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> IDHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />