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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> Mccampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www rnrc bell corn ]-mad maul campbell com <br /> Advanced GeoEnvironmental,Inc Client Project ID Waterloo F/F-Start up Date Sampled 05/15/03 <br /> 837 Shaw Road Date Received 05/16/03 <br /> Client Contact Bill Little Date Extracted 05/16103-05122/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 05/16/03-05/22/03 <br /> MTBE and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW 8260E Work Order 0305251 <br /> Lab ID 0305251-005B � <br /> Client ID EW4-Influent <br /> Reporting Limit for <br /> DF=l <br /> Matrix W � �- ------ - <br /> DF1000I S W <br /> Compound Concentration ug/kg µg/L <br /> Benzene 3600 NA 05 <br /> Ethylbenzene ND<500 NA 05 <br /> Methyl-t-butyl ether(MTBE) 23,000 NA 0 5 <br /> Toluene ND<500 NA 0 5 <br /> Xylenes ND<500 NA 0 5 <br /> Surrogate Recoveries <br /> %55t —_ ­ <br /> 823 <br /> %SS2 92 7 <br /> %SS3 878 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples to ug/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br />' organic content <br /> DHS Certification No 1644 Angela Rydebus,Lab Manager <br />