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cb LABORATORY NUMBER: 206750 PAGE 2 OF 3 CLIENT: APPLIED CONSULTANTS DATE SAMPLED: 05/17/93 ' DATE ANALYZED: SEE BELOW TOTAL PETROLEUM HYDROCARBONS AS GASOLINE ' MATRIX: SOLID METHOD: DHS LUFT PROCEDURE (MOD. 8015) EXTRACTION: EPA 5030 PURGE AND TRAP 1 - - - - - - - ` - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - LAB ID SAMPLE ID RESULT DATE SUR. QC ID ' (ug/Kg) ANALYZED % REC BATCH - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 004 B4-D20 ND 05/21 99 A ' 005 B4-D25 ND 05/21 99 A 006 B4-D30 ND 05/22 100 B 007 B4-D35 ND 05/22 ill B 008 B4-D40 TR -300 05/21 103 A 009 B4-D45 760 05/21 108 A 010 B4-D50 ND 05/21. 97 A Oil B4-D55 ND 05/22 102 A ' 012 B4-D60 700 , 000-a 05/22 96 A 013 B4-D65 9 , 500-b 05/22 100 B 014 B4-D70 570 05/22 109 B METHOD BLANK A ND 05/21 1.1.0 A METHOD BLANK B ND 05/22 98 B ' DETECTION LIMIT: 500 a = 1 : 500 DILUTION RUN ON 05/22/93 . b = 1 : 5 DILUTION RUN ON 05/22/93 . - - - - - - - - - - - - - - - - - - - - - - - - - - -QUALITY CONTROL SUMMARY_ - _ - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ' SURROGATE: a,a,a-Trifluorotoluene - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - MS/MSD DATA: SAMPLE NUMBER: 206749-005 ANLYSIS DATE: 05/21./93 ' MS/MSD DATA: SAMPLE NUMBER: 206750-006 ANLYSIS DATE: 05/22/93 SPIKE SPIKE DUP. AVG. QC ID REC. % REC. RPD BATCH ' SPIKE/SPIKE DUPLICATE RECOVERY: 105 107 2 A SPIKE/SPIKE DUPLICATE RECOVERY: 96 104 8 B