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1 <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http llwww mccampbell cam E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID Top Filling Date Sampled 04/10/2000 <br /> 4005 North Wilson Way Date Received 04/13/2000 <br />' Stockton, CA 95205 Client Contact Tun Cuellar Date Extracted 04/13/2000 <br />' Client P O Date Analyzed 04/15-04/19/2000 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 35857 <br /> Client ID CPTIA-86' <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone 16i ND<10 trans-1,3-Dichloropropene NIK10 <br /> Benzene 77 Ethylene dibromide ND<10 <br /> Bromobenzene ND<10 Ethylbenzene 120 <br /> Bromachloromethane ND<10 Hexachlorobutadiene ND<10 <br />' Bromodichloromeihane ND<10 lodomethane ND<10 <br /> Bromoform ND<10 Isopropylbenzene ND<10 <br /> Bromomethane ND<10 p-Isopropyl toluene ND<10 <br />' n-Butyl benzene 18 Methyl butyl ketoneND<10 <br /> sec-Butyl benzene ND<10 Methylene Chlonde" ND<10 <br /> tent-Butyl benzene ND<10 Methyl ethyl ketone ND<10 <br /> Carbon Disulfide ND<10 Methyl isobutyl ketone`s ND<10 <br /> Carbon Tetrachloride NIK10 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<10 Naphthalene 27 <br /> Chloroethane ND<10 n-Propyl benzene 26 <br /> 2-Chloroethyl Vinyl Ether` ND<10 Styrene ND<10 <br />' Chloroform ND<10 1,1,1,2-Tetrachloroethane ND<10 <br /> Chloromethane ND<10 1,1,2,2-Tetrachloroethane ND<10 <br /> 2-Chlorotoluene ND<10 Tetrachloroethene ND<10 <br /> 4-Chlorotoluene ND<l0 Toluene' 250 <br />' Dibromochloromethane ND<10 1 2,3-Tnchlorobenzene ND<10 <br /> 1,2 Dibromo-3-chloropropane ND<10 1,2,4 Trichlorobenzene ND<10 <br /> Dtbromomethane ND<10 1,1,1-Trichloroethane ND<10 <br /> 1,2-Dichlorobenzene ND<10 1,1,2-Trichloroethane ND<10 <br /> I 1,3-Dichlorobenzene ND<10 Tnehloroethene ND<10 <br /> 1,4-Dichlorobenzene ND<10 Trichlorofluoromethane ND<10 <br /> Dichlorodifluoromethane ND<10 1,2,3-Tnehloropropane ND<10 <br /> l,l-Diehl oroethane ND<10 1 2 4-Trimethylbenzene 200 <br />' 1 2-Dichloroethane ND<10 1 3 5-Trimeihylbenzene ND<10 <br /> 1,1-Dichloroethene ND<10 Vinyl Acetate'"' ND<10 <br /> cis-1,2-Dichloroethene ND<]0 Vinyl Chloride'" ND<10 <br /> trans-l,2-Dichloroethen e ND<10 Xylenes,total 101 400 <br />' 1,2-Dichloropropane ND<10 Comments <br /> 1,3-Dichloropropane ND<10 Surrogate Reco\eries(%) <br /> 2,2-Dichloropropane ND<10 Dibromofluoromethane 120 <br /> I,1-Dichloropropene ND<10 Toluene-d8 104 <br /> cis 1,3-Dichloropropene ND<10 4-Bromotluorobenzene 97 <br /> eater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,Napor samples 0 5 ug/L solid and sludge samples 5 ug/kg,wipes 0 Zug/wipe <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone (c) (2-chloroethoxy)ethene, (d)2-hexanone (e)dichloromethane, (f) 2-butanone, (g) 4-methy1-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethcne,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />