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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> ® McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hftR//www_mccampbell com E-mail mam@mccampbell com <br /> Advanced GeoEnvironmental CIient Project ID Top Filling Date Sampled 03/06/2002 <br /> 837 Shaw Road Date Received 03/08/2002 <br /> IStockton, CA 95215 Client Contact Tun Cuellar Date Extracted 03108-03/1412002 <br /> Client P O Date Analyzed 03108-03/14/2002 <br /> Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> I Lab ID 0203139-005 0203139-006 0203139-007 0203139-008 <br /> Reporting Limit <br /> Client 1D MW5/030602 MW6a/030602 MW6b/030602 MW6c/030602 <br /> Matm W W W W SW <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND<2500 ND<25 ND 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND<2500 ND<25 ND so 1 0 <br /> Methyl tert-Butyl Ether(MTBE) ND 31,000 460 ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND<2500 ND<25 ND so 10 <br /> tert-Butanol 140 ND<13,000 ND<1300 ND 25 50 <br /> Methanol ND ND<1,300,000 ND<l30,000 ND 2500 500 <br /> Ethanol ND ND<130,000 ND<13,000 ND 250 50 <br /> I <br /> Surrogate Recoveries(%) <br /> Dibramofluoromethane 106 111 104 107 <br /> IComments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644Edward Hamilton,Lab Director <br />