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I110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925.798-1620 Fax 925-798-1622 <br /> JJ http//www=22Mpbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Top Filling <br /> Date Sampled 05/29/01 <br /> 837 Shaw Road Date Received 06/01/01 <br /> IStockton, CA 952I5 Client Contact Tort Cuellar Date Extracted 06/01-06106101 <br /> Client P O Date Analyzed 06/01-06/06/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 68781 68782 68783 68784 <br /> MW1/ MW2/ MW3/ MW4/ Reporting Lirtnt <br /> Client ID 052901 052901 052901 052901 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND<10 ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND<10 ND 50 1 0 <br /> Methyl tert-Butyl Ether(MTBE) 130 15 250 ND 50 1 0 <br /> lie <br /> tert-Amyl Methyl Ether(TAME) 68 ND ND<10 ND 50 10 <br />' tert-Butanol ND ND ND<50 ND 25 50 <br /> Methanol ND ND ND<5000 ND 1000 500 <br /> Ethanol ND ND ND<500 ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoramethane 106 108 107 110 <br />' Comments <br /> 'water samples are reported in ug/L,soil and sludge samples in ug/kg,vnpes in ughope and ail TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,(I)sample diluted due to <br /> high organic content <br /> IDHS Certification No 1644 Jlk—Edward Hamilton, Lab Director <br /> I <br />