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1 <br /> i CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive Atwater CA 95301 Phone (209) 384-2930 <br /> iCertificate#2079 Fax (209) 384-1507 <br /> Advanced GeoEnvironmental, Inc Client Protect ID Top Filling Sampled 5-29-01 <br /> i of Northern California Reference Number 3790 Received 5-31-01 <br /> 837 Shaw Road Sample Description Water Extracted 6-8-01 <br /> Stockton,CA 95215 Sample Prep/Analysis Method EPA 5030/8015, 8020 Analyzes! 6-8-01 <br /> Attn Tim Cuellar Lab Numbers 3790-1W,2W, 3W,4W 5W Reported 6-13-01 <br /> i <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br />' WITH BTEX DISTINCTION <br /> i ANALYTE REPORTING LIMIT SAMPLE 1D SAMPLE ID SAMPLE lD SAMPLE ID SAMPLE ID <br /> MW1 MW2 MW3 MW4 MW5 <br /> 052901 052901 052901 052901 052901 <br /> (ug/L) (ug1L) (uglL) (ug/L) (ug/L) (ug/L) <br /> MTBE 050 120 ND 240 NO ND <br /> BENZENE 050 40 270 2900 41 110 <br /> TOLUENE 050 48 21 200 36 12 <br /> . ETHYL BENZENE 050 16 21 170 11 19 <br /> TOTAL XYLENES 050 11 63 460 85 100 <br /> GASOLINE RANGE <br /> HYDROCARBONS 50 140 1000 8000 63 1500 <br /> Report Limit Multiplication Factor 1 1 1 1 10 <br /> Report Limit Multiplication Factor MTBE only 10 <br /> Report Limit Multiplication Factor Benzene only 10 200 <br /> Surrogate%Recovery FID 104%IPID 994A FID 132/.IPiD 109% NA FID 131%IPID 986% FID 138%lPID 115A <br /> I <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> Anaiytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantdation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST APPROVED BY <br /> Clan J Cane Ja s C Phillips rr <br /> aboratory Director <br />