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I <br /> CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> ICertificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Top Filling Sampled 07-24-03 <br /> of Northern California Reference Number 5923 Received 07-25-03 <br /> 837 Shaw Road Sample Description Soil Extracted 07-25-03 <br /> Stockton,CA 95215 Sample Prep/Analysis Method EPA 503018260 Analyzed 07-26-03 <br /> Attn Tim Cuellar Lab Numbers 5923-1 S, 2S 3S Reported 08-18-03 <br /> r <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GC/MS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID <br /> LIMIT EW2-25 EW2-40 EW2-55 <br />' m /K m 1K m !K m !K <br /> FUEL QXYGENATES <br />' Methyl tert-Butyl Ether(MTBE) 0 010 NO NO 0 047 <br /> Di-isopropyl Ether (DIPS) 0 010 NO NO NO <br />' Ethyl tert-Butyl Ether (ETBE) 0 010 NO NO NO <br /> tert-Amyl Methyl Ether(TAME) 0 010 ND NO ND <br />' tert-Butanol(TBA) 0 800 NO ND NO <br /> VOLATILE HALOCARBONS <br />' 1 2-Dichloroethane (1,2-DCA) 0 010 NO NO 0 019 <br /> Ethylene Dibromide (EDB) 0 010 ND NO NO <br />' Report Limit Multiplication Factor 1 1 1 <br /> 1 <br />' Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 615% 980% 775% <br /> Toluene-d8 631% 705% 832% <br />' Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligrams per kilog parts per million(ppm) <br /> SANALYST APPROVED BY <br />' Clan J Cone Ja hillips <br /> or Director <br />