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jjLancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Poke PO Box 12425 L8ncasler PA 17605.2425•717 E56 2300 Fax 717-6562681 www lancaslerlabs corn <br /> Page 2 of 4 <br /> Quality Control Summary <br /> Client Name Chevron c/o SECOR Group Number 976204 <br /> Reported 02/09/06 at 12 56 PM <br /> Sample Matrix Quality Control <br /> Unspiked IUNSPK) = the sample used in conjunction with the matrix spike <br /> Backarouno (EKG) = the sample used in con3unction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPA <br /> Analysis Name %REC %RBC LSmitE RPD MAX Con c Conc RPD Max <br /> Batch number 06032A16F Sample number(s) 4699008 UNSPK P699003 <br /> TPN-GRO - Waters 117 63-154 <br /> Batch number 060330017E Sample number(s) 4699009-4699013 UNSPK P697972 <br /> Methanol (by Direct In]ection) 96 104 66-13- 8 20 <br /> Batch number 06033A16A Sample number(s) 4699009-4699015 UNSPK P699039 <br /> TPH-GRO - Waters 326 63-154 <br /> Batch number 060380002A Sample numbers) 4699014-4699015 UNSPK 4699014 <br /> Methanol (by Direct Inaection) 104 100 66-13- 4 20 <br /> Batch number P060352AP Sample number(s) 4699009-4699013 UNSPK P700904 <br /> Ethanol 93 105 26-162 12 30 <br /> 0 h <br /> yl Tertiary Butyl Ether 97 99 69-134 2 30 <br /> ..propyl ether 81 62 75-130 1 30 <br /> 1 t-butyl ether 83 e6 78-115 3 30 <br /> t-Amyl methyl ether 88 90 72-125 2 30 <br /> t-Butyl alcohol 90 103 56-134 13 30 <br /> Benzene 91 92 E3-22E 1 30 <br /> 1,2-Dichloroethane 89 93 4 30 <br /> Toluene 91 93 63-127 2 30 <br /> 1,2-Dibromoethane Be 8E 7E-120 1 30 <br /> Ethylbenzene 92 94 62-129 2 30 <br /> Xylene (Total) 92 93 82-130 0 30 <br /> Batch number Z060371AA Sample numberts) 4699008 UNSPK P696476 <br /> Methyl Tertiary Butyl Ether 120 114 69-127 5 30 <br /> Benzene 110 108 63-22E 1 30 <br /> Toluene 115 113 E3-127 1 30 <br /> Ethylbenzene 114 112 62-129 2 30 <br /> Xylene (Total) 113 11_ 82-130 1 30 <br /> Batch number Z06O3E3AA Sample number(s) 4699014-4699015 UNSPK P696409 <br /> Ethanol 95 99 34-161 3 30 <br /> Methyl Tertiary Butyl Ether 116 113 69-127 3 30 <br /> ai-Isopropyl ether 102 105 75-130 3 30 <br /> Ethyl t-butyl ether 105 30E 78-119 3 30 <br /> t-Amyl methyl ether 106 105 72-125 - 30 <br /> t-Butyl alcohol 96 97 64-130 3 30 <br /> Benzene SOE 109 63-128 1 30 <br /> 1 2-Dichloroethane 113 3I5 70-14- 2 30 <br /> Toluene 112 113 83-127 1 30 <br /> 1 2-Dibromoetnane 102 103 76-120 1 30 <br /> Ethylbenzene 111 112 62-129 1 30 <br /> Xylene (Total) 111 112 62-130 1 30 <br /> *- Outside of specification <br /> The result for one or both determinations was le"than five times the LOQ <br /> The background result was more than four times the spike added <br />