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Analysis • • <br /> Lancaster Laboratories Page I of 3 <br /> . WheCe%Titya wren€rol Summary <br /> Client Name Chevron Products Company Group Number 804247 <br /> Reported 04/25/02 at 11 58 AM <br /> Laboratory Complmance Quality Control <br /> Blank Blank Report LCS LC5D LCS/LCSD <br /> Analysers Name Result MDL Unerta %REC %REC Lxmi.ts RPD RPD Max <br /> Batch number 02107A33A Sample number(s) 3806155-3806156 <br /> TPH-GRO - Soils N D 1 mg/kg 85 75-117 <br /> Batch number. 02107A33B Sample number(s) 3806159-3806162 <br /> TPH-GRO - Soils N D 1 mg/kg 85 75-117 <br /> Batch number 021130016A Sample number(s) 3806155-3806162 <br /> Ethanol (by Direct In3ection) N D 200 ug/kg 88 76--115 <br /> Methanol (by Direct In3ection) N D 200 ug/kg 80 79-117 <br /> Batch number D021091AA Sample numbers) 3806155-3806162 <br /> Methyl t-butyl ether N D 1 ug/kg 97 75-135 <br /> di-Isopropyl ether N D I ug/kg 102 73-127 <br /> Ethyl t-butyl ether N D 1 ug/kg 97 73-135 <br /> t-Amyl methyl ether N D I ug/kg 93 71-132 <br /> t-Butyl alcohol N D 20 ug/kg Bl 52-158 <br /> Benzene N D 1 ug/kg 105 85-125 <br /> Toluene N D 1 ug/kg 102 84-125 <br /> Ethylbenzene N D 1 ug/kg 102 86-127 <br /> Xylene (Total) N D 1 ug/kg 103 87-127 <br /> Sample Matrix Qual3.ty Control <br /> MS MSD M9/MSD RPD BKG DUP DUP DuP <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Cone Cone RPD Max <br /> Batch number 02107A33A Sample number(s) 3806155-3806158 <br /> TPH-GRO - Soils 70 70 44-116 0 30 <br /> Batch number 02107A33B Sample number(s) 3806159-3806162 <br /> TPH-GRO - Soi1s 70 70 44-116 0 30 <br /> Batch number- 021130016A Sample number(s) 3806155-3806162 <br /> Ethanol (by Direct Injection) 76 76 60-140 0 20 <br /> Methanol (by Direct In3ection) 68 72 60-140 6 20 <br /> Batch number- D021091AA Sample number(s) 3806155-3806162 <br /> Methyl t-butyl ether 85 87 52-150 2 30 <br /> di-Isopropyl ether 94 97 57-139 3 30 <br /> Ethyl t-butyl ether 67 90 53-148 4 30 <br /> t-Amyl methyl ether 83 84 52-144 2 30 <br /> t-Butyl alcohol 70 71 17-199 2 30 <br /> Benzene 96 98 43-151 2 30 <br /> Toluene 99 100 27-163 1 30 <br /> Ethylbenzene 97 97 30-158 0 30 <br /> Xylene ('Total) 96 97 46-158 1 30 <br /> *-Outside of specification <br /> 46 The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br /> Lancaster Laboratories,Inc <br /> MEMBER 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster,PA 17605-2425 <br /> 717 656-2300 Fax 717-656-2681 2216 Rev 9/11/00 <br />