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t i Report Number 38662 QC Report Matrix Spike/Matrix Spike Duplicate Date 6/15/2004 Project Name Former Beacon 12419 Project Number 1419.47 i Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 38724-03 <0 50 400 400 374 376 uglL EPA 8260E 6112104 936 941 0 572 70-130 25 Toluene 38724-03 <0 50 400 400 387 381 uglL EPA 8260B 6112104 967 952 162 70-130 25 Tert-Butanol 3872403 <5 0 200 200 204 193 ug1L EPA 8260B 6112104 102 963 570 70-130 25 Methyl-t-Butyl Ether 38724-03 4 8 400 400 425 432 ug/L. EPA 8260E 6112104 941 958 1 79 70-130 25 Benzene 38662-04 420 400 400 450 447 ug1L EPA 82606 6110104 871 803 814 70-130 25 Toluene 38662-04 68 400 400 474 477 ug/L EPA 82608 6/10104 101 102 0 909 70-130 25 Tert-Butanol 38662-04 6 8 200 200 210 214 uglL EPA 8260B 6110104 102 103 167 70-130 25 Methyl-t-Butyl Ether 38662-04 073 400 400 456 458 ug/L. EPA 82606 6110104 112 113 0 454 70-130 25 I Benzene 38661-04 <0 50 400 400 397 384 uglL EPA 8260B 6111104 992 960 327 70-130 25 Toluene 38661-04 <0 50 400 400 381 386 ug/L EPA 8260B 6111104 953 964 121 70-130 25 Tert-Butanol 38661-04 <5 0 200 200 201 200 uglL EPA 8260B 6111104 100 999 0 499 70-130 25 Methyl-t-Butyl Ether 38661-04 <0 50 400 400 430 426 uglL EPA 8260B 6111/04 108 106 0 958 70-130 25 Benzene 38723-01 <0 50 400 400 351 361 uglL EPA 82606 6114104 878 902 265 70-130 25 Toluene 38723-01 <0 50 400 400 354 36 3 ug1L EPA 82606 6114104 886 907 235 70-130 25 Teri-Butanol 38723-01 <5 0 200 200 177 190 ug/L EPA 82606 6114104 88 7 95 0 685 70-130 25 Methyl-t-Butyl Ether 38723-01 42 400 400 776 780 ug/L EPA 82606 6114104 882 894 141 70-130 25 KIFF ANALYTICAL, LLC Approved By ,toe iff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800