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Report Number 28609 QC Report Matrix Spike/Matrix Spike Duplicate Date 9/26/2002 Protect Name Former Beacon 12419 Protect Number 1419.45 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 28609-11 120 200 198 304 299 ug/L EPA 8260B 9124102 937 922 1 60 70-130 25 Toluene 28609-11 110 200 198 294 289 ug/L EPA 8260B 9124102 908 890 196 70-130 25 Tert-Butanol 28609-11 <50 1000 990 1010 1020 ug/L EPA 8260B 9124/02 101 103 1 87 70-130 25 Methyl-t-Butyl Ether 28609-11 <0 50 200 198 207 208 ug/L EPA 82608 9124102 104 105 132 70-130 25 Benzene 28601-01 2 7 400 400 365 35 0 ug/L EPA 8260B 9119102 844 808 436 70-130 25 Toluene 28601-01 24 400 400 34 3 32 6 ug/L EPA 8260B 9119/02 798 755 554 70-130 25 Tert-Butanol 28601-01 <50 200 200 209 207 ug/L EPA 8260B 9119/02 105 104 110 70-130 25 Methyl-t-Butyl Ether 28601-01 <0 50 400 400 322 323 ug/L EPA 8260B 9119102 804 808 0 496 70-130 25 Benzene 28609-04 <0 50 400 400 354 339 ug/L EPA 8260B 9119102 88 6 848 444 70-130 25 Toluene 28609-04 <0 50 400 400 354 335 ug/L EPA 8260B 9119102 884 838 537 70-130 25 Teri-Butanol 28609-04 <5 0 200 200 191 189 ug/L EPA 8260B 9119102 95 5 94 6 0 936 70-130 25 Methyl-t-Butyl Ether 28609-04 <0 50 400 400 291 288 ug/L EPA 82608 9119/02 727 71 9 104 70-130 25 Benzene 28665-04 <0 50 400 400 41 7 422 ug/L EPA 8260B 9/20102 104 106 1 17 70-130 25 Toluene 28665-04 <0 50 400 400 455 455 ug/L EPA 8260B 9120102 114 114 0 154 70-130 25 Tert-Butanol 28665-04 <5 0 200 200 215 216 ug/L EPA 82608 9120/02 108 108 0 107 70-130 25 Methyl-t-Butyl Ether 28665-04 14 400 400 56 5 61 2 ug/L EPA 8260B 9120102 106 118 105 70-130 25 Approved By Jbel Kiff KIFF ANALYTICAL, LLC I } 720 Olive Drive, Suite D Davis, CA 95616 530-297-4800