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Alpha Analytical, Inc. Analytical Report <br /> (775 ) 355 - 1044 / (775 ) 355 - 0406 FAX / 1 - 800-283 - 1183 <br /> 255 Glendale Ave . - Suite 21 - Sparks , Nevada 89431 -5578 WO# : BBA2001009 <br /> fro""1e"�9� Report Date : 1/8/2020 <br /> CLIENT : Broadbent & Associates , Inc . Collection Date : 1 /3 /2020 9 : 33 : 00 AM <br /> Project: 19 -08 - 161 /Pilot Flying J #618 UST Removal <br /> Lab ID : 2001009- 01 Matrix: SOIL <br /> Client Sample ID SP- 1 <br /> Analyses Result RL Qual Units Date Analyzed Method <br /> Beryllium (Be) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Vanadium (V) 36 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Chromium (Cr) 15 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Cobalt (Co) 3 .9 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Nickel (Ni) 9 .9 4 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Copper (Cu) 9 .6 4 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Zinc (Zn) ND 40 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Arsenic (As) ND 2 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Selenium (Se) ND 4. 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Molybdenum (Mo) ND 2. 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Silver (Ag) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Cadmium (Cd) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Antimony (Sb) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Barium (Ba) 83 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Mercury ( Hg) ND 0.50 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Thallium (TI) ND 2 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Lead (Pb) 3 .6 2 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Naphthalene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Acenaphthylene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Acenaphthene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Fluorene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Phenanthrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Anthracene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Fluoranthene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Pyrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Benzo(a) anthracene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Chrysene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Benzo(b&k)fluoranthene, isomeric pair ND 50 pg/Kg 1 /6/2020 PNAs by EPA 8270SiM <br /> Benzo(a)pyrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Indeno( 1 , 2 , 3-cd) pyrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Dibenz(a, h) anthracene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Benzo(g , h , i) perylene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Surr: 2-Fluorobiphenyl 108 52- 130 % Rec 1 /6/2020 PNAs by EPA 8270SIM <br /> Surr: 4-Terphenyl-d14 86 54- 158 % Rec 1 /6/2020 PNAs by EPA 8270SIM <br /> TPH-E (DRO) 12 5 .0 L mg/Kg 1 /7/2020 TPH - E by EPA 8015C <br /> TPH-E (ORO) 160 10 mg/Kg 1 /7/2020 TPH - E by EPA 8015C <br /> Surr: Nonane 96 66- 134 %Rec 1 /7/2020 TPH -E by EPA 8015C <br /> TPH -P (GRO) ND 1 . 0 mg/Kg 1 /6/2020 TPH -P by EPA 8015C <br /> Surr: 1 , 2-Dichloroethane-d4 71 70- 130 % Rec 1 /6/2020 TPH-P by EPA 8015C <br /> Surr: Toluene-d8 113 70- 130 % Rec 1 /6/2020 TPH-P by EPA 8015C <br /> Surr: 4-Bromofluorobenzene 123 70- 130 % Rec 1 /6/2020 TPH-P by EPA 8015C <br /> Chloromethane ND 40 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> Vinyl chloride ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> Chloroethane ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> Bromomethane ND 40 pg/Kg 1 /6/2020 VOCs by EPA 8260B Page 2 of 23 <br /> Trichlorofluoromethane ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> 1 , 1 -Dichloroethene ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br />