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Alpha Analytical, Inc. Analytical Report <br /> ` (775 ) 355 - 1044 / (775 ) 355 -0406 FAX / 1 - 800 -283 - 1183 <br /> 255 Glendale Ave . - Suite 21 - Sparks, Nevada 89431 -5578 WO# : BBA2001009 <br /> Report Date : 1 /8/2020 <br /> CLIENT : Broadbent & Associates , Inc . Collection Date : 1 /3/2020 10 : 06 : 00 AM <br /> Project : 19 -08 - 161 /Pilot Flying J #618 UST Removal <br /> Lab ID : 2001009- 04 Matrix: SOIL <br /> Client Sample ID T2 <br /> Analyses Result RL Qual Units Date Analyzed Method <br /> Beryllium (Be) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Vanadium (V) 37 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Chromium (Cr) 13 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Cobalt (Co) 4.2 2 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Nickel (Ni) 9 .2 4 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Copper (Cu) 8. 1 4 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Zinc (Zn) ND 40 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Arsenic (As) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Selenium (Se) ND 4 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Molybdenum (Mo) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Silver (Ag) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Cadmium (Cd) ND 2 .0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Antimony (Sb) ND 2 .0 mg/Kg 117/2020 Metals by EPA 6020 <br /> Barium (Ba) 51 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Mercury (Hg) ND 0 . 50 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Thallium (TI) ND 2 . 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Lead (Pb) ND 2. 0 mg/Kg 1 /7/2020 Metals by EPA 6020 <br /> Naphthalene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Acenaphthylene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Acenaphthene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Fluorene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Phenanthrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Anthracene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Fluoranthene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Pyrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Benzo(a)anthracene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Chrysene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SiM <br /> Benzo(b&k)fluoranthene, isomeric pair ND 50 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Benzo(a) pyrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Indeno(1 ,2 , 3-cd) pyrene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Dibenz(a, h) anthracene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Benzo(g , h , i) perylene ND 25 pg/Kg 1 /6/2020 PNAs by EPA 8270SIM <br /> Surr: 2- Fluorobiphenyl 110 52-130 %Rec 1 /6/2020 PNAs by EPA 8270SIM <br /> Surr: 4-Terphenyl-d14 78 54- 158 %Rec 1 /6/2020 PNAs by EPA 8270SIM <br /> TPH -E (DRO) ND 5 .0 mg/Kg 1 /7/2020 TPH-E by EPA 8015C <br /> TPH -E (ORO) ND 10 mg/Kg 1 /7/2020 TPH- E by EPA 8015C <br /> Surr: Nonane 98 66- 134 % Rec 1 /7/2020 TPH-E by EPA 8015C <br /> TPH -P (GRO) ND 1 . 0 mg/Kg 1 /6/2020 TPH -P by EPA 8015C <br /> Surr: 1 , 2- Dichloroethane-d4 70 70- 130 %Rec 1 /6/2020 TPH -P by EPA 8015C <br /> Surr: Toluene-d8 118 70- 130 %Rec 1 /6/2020 TPH-P by EPA 8015C <br /> Surr: 4-Bromofluorobenzene 124 70- 130 % Rec 1 /6/2020 TPH-P by EPA 8015C <br /> Chloromethane ND 40 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> Vinyl chloride ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> Chloroethane ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> Bromomethane ND 40 pg/Kg 1 /6/2020 VOCs by EPA 8260B Page 8 of 23 <br /> Trichlorofluoromethane ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br /> 1 , 1 - Dichloroethene ND 20 pg/Kg 1 /6/2020 VOCs by EPA 8260B <br />