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l / <br /> i <br /> **;7 SPL BATCH CUALITT CONTROL REPORT ** PACE 1 <br /> METHOD 8020*** <br /> Batch Id: HP_U950109172700 <br /> - Lnits: +tp/Kg <br /> LA00R.AT0RT C _�T,R2L S A N e L E _ <br /> L <br /> S P I K E Method Spike Blank Spike OC Limits(") <br /> C O M P O U N D S Blank Result Added Result Recovery (Mandatory) <br /> <2> -c1> <1> % % Recovery Range <br /> Benzene ND 50 47 94.0 51 - 125 <br /> Toluene ND 50 -47 94.0 52 126 <br /> EthylBenzene ND 50 47 94.0 53 125, <br /> 0 xylene ND 50 46 92.0 32 - 160 <br /> N & P xylene ND 100 92 92.0 32 - 160 <br /> S P I K E Sample Spike Matrix Spike Matrix Spike MS/MSD 4C Limits("*)C O K P 0 U N D S Results Added DUDIiCate Relative X (Advisory) <br /> Result Recovery 'Result Recovery Difference RPD <br /> c22., t3> cl> 4> <1> <5> Max. I Recovery Range <br /> r <br /> Benzene ND 20 19 95.0 20 100 5.13 33 47 - 143 <br /> Toluene 1 20 21 100 21 100 0 35 46 - 148 <br /> EthylBenzene ND 20 20 100 21 105 4.88 40 32 - 151 <br /> 0 Xylene NDI 20 19 95.0 20 100 5.13 24 18 - 144 <br /> N A P Xylene HD 40 37 92.5 38 95.0 2.67 23 25 - 139 <br /> Analyst: LFD * = Values Outside OC Range <br /> Sequence Date: 01/09/95 NC a Not Calculated (Sample exceeds spike by factor of 4 or more) <br /> SPL ID of sample spiked: 9501053-ZIA ND a Not Detected/Below Detection Limit <br /> Sample File ID: U_368.TXO % Recovery = [( 02, - <2> ) / <3> I x 100 <br /> Method Blank File 10: LCS % Recovery = (<1> / <3> ) x 100 <br /> Blank Spike File ID: U-358.TXO Relative Percent Difference = 1(<4> - <5> I / C(<4> * <5)-- ) x 0.51 x 100 <br /> Matrix Spike File ID: U_360.TXO (**) = Source: SPL-Houston Historical Data r <br /> Matrix Spike Duplicate File ID: U_361.TX0 (***) = Source: SPL-Houston Historical Data <br />�l <br /> _SAMPLES IN BATCH(SPL ID): 9501235-04A 9501235-09A 9501235-07A 9501235-IOA <br /> 9501235-08A 9501235-12A 9501235-11A 9501235-06A <br /> 9501235-05A 9501231-07A 9501231-06A 95OJ231-OSA <br /> 9501231-03A 9501231-02A 9501231-OIA 9501053-23A <br /> 9501053-22A 9501053-24A 9501053-21A <br /> Idelis Wltiams OC Officer <br />