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Report Number 43856 <br /> Date 6/10/2005 <br /> • ANALYTICAL LLC <br /> Project Name Restructure Petroleum-Stockton <br /> Project Number RPMS0966 <br /> Sample VW-1 Matrix Water Lab Number 43856-19 <br /> Sample Date 5/17/2005 <br /> Method <br /> Measured Reporting Analysts Date <br /> Parameter Value Limit Units Method Anal zed <br /> Benzene 7100 10 ug/L EPA 8260B 5/20/2005 <br /> Toluene 73 10 ug/L EPA 8260B 5/20/2005 <br /> Ethylbenzene 220 10 ug/L EPA 8260B 5/20/2005 <br /> Total Xylenes 550 10 ug/L EPA 8260B 5/20/2005 <br /> Methyl-t-butyl ether(MTBE) 140 10 ug/L EPA 8260B 5/20/2005 <br /> Diisopropyl ether(DIPE) < 10 10 ug/L EPA 8260B 5/20/2005 <br /> Ethyl-t-butyl ether(ETBE) < 10 10 ug/L EPA 8260B 5/20/2005 <br /> Tert-amyl methyl ether(TAME) < 10 10 ug/L EPA 8260B 5/20/2005 <br /> Tert-Butanol 56 50 ug/L EPA 8260B 5/20/2006 <br /> Methanol < 1000 1000 ug/L EPA 82608 5/20/2005 <br /> Ethanol < 100 100 ug/L EPA 8260B 5/20/2005 <br /> 1,2-Dichloroethane < 10 10 ug/L EPA 8260B 5/20/2005 <br /> 1,2-Dibrornoethane < 10 10 ug/L EPA 8260B 5/20/2005 <br /> TPH as Gasoline 18000 1000 ug/L EPA 82606 5/20/2005 <br /> Toluene-d8 (Surr) 997 % Recovery EPA 8260B 5/20/2005 <br /> 4-Bromofluorobenzene (Surr) 96 0 % Recovery EPA 8260B 5/20/2005 <br /> Approved By Jo I iff <br /> 2795 2nd St , Suite 300 Davis, CA 95616 530-297-4800 <br />