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QC Sample Results Client: ProTech Consulting and Engineering Job ID: 720-92770-1 Project/Site: SRVHS Stockpile Method: 8270C - Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) (Continued) Lab Sample ID: 720-92770-5 MS Client Sample ID: SP-1A,B,C,D Matrix: Solid Prep Type: Total/NA Analysis Batch: 265019 Prep Batch: 264883 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,2-Dichlorobenzene ND 2.55 1.28 mg/Kg 50 39-110 2-Methylphenol ND 2.55 1.59 mg/Kg 62 50-110 Methylphenol,3&4 ND 2.55 1.45 mg/Kg 57 51-110 N-Nitrosodi-n-propylamine ND 2.55 1.42 mg/Kg 56 46-110 Hexachloroethane ND 2.55 1.28 mg/Kg 50 40-110 Nitrobenzene ND 2.55 1.51 mg/Kg 59 45-110 Isophorone ND 2.55 1.51 mg/Kg 59 49-110 2-Nitrophenol ND F1 2.55 0.613 F1 mg/Kg 24 41-105 2,4-Dimethylphenol ND 2.55 1.44 mg/Kg 57 52-100 Bis(2-chloroethoxy)methane ND 2.55 1.41 mg/Kg 55 46-110 2,4-Dichlorophenol ND 2.55 1.42 mg/Kg 56 49-100 1,2,4-Trichlorobenzene ND 2.55 1.46 mg/Kg 57 43-110 Naphthalene ND 2.55 1.38 mg/Kg 54 44-110 4-Chloroaniline ND F1 2.55 0.901 F1 mg/Kg 35 42-110 Hexachlorobutadiene ND 2.55 1.56 mg/Kg 61 44-110 4-Chloro-3-methylphenol ND 2.55 1.69 mg/Kg 66 58-104 2-Methylnaphthalene ND 2.55 1.50 mg/Kg 59 49-110 Hexachlorocyclopentadiene ND F1 2.55 ND F1 mg/Kg 0 24-106 2,4,6-Trichlorophenol ND F1 2.55 0.626 F1 mg/Kg 25 50-105 2,4,5-Trichlorophenol ND F1 2.55 1.00 F1 mg/Kg 39 53-106 2-Chloronaphthalene ND 2.55 1.46 mg/Kg 57 52-110 2-Nitroaniline ND 2.55 1.51 mg/Kg 59 51-115 Dimethyl phthalate ND 2.55 1.50 mg/Kg 59 56-103 Acenaphthylene ND 2.55 1.44 mg/Kg 56 53-102 3-Nitroaniline ND 2.55 1.53 mg/Kg 60 50-110 Acenaphthene ND 2.55 1.43 mg/Kg 56 53-103 2,4-Dinitrophenol ND F1 5.10 ND F1 mg/Kg 0 10-115 4-Nitrophenol ND F1 5.10 2.13 F1 mg/Kg 42 54-117 Dibenzofuran ND 2.55 1.46 mg/Kg 57 55-101 2,4-Dinitrotoluene ND 2.55 1.40 mg/Kg 55 54-115 2,6-Dinitrotoluene ND 2.55 1.45 mg/Kg 57 54-107 Diethyl phthalate ND 2.55 1.62 mg/Kg 64 56-107 4-Chlorophenyl phenyl ether ND 2.55 1.67 mg/Kg 66 57-106 Fluorene ND 2.55 1.43 mg/Kg 56 54-103 4-Nitroaniline ND 2.55 1.84 mg/Kg 72 49-115 2-Methyl-4,6-dinitrophenol ND F1 5.10 ND F1 mg/Kg 0 31-122 N-Nitrosodiphenylamine ND 2.55 1.63 mg/Kg 64 56-104 4-Bromophenyl phenyl ether ND 2.55 1.48 mg/Kg 58 53-104 Hexachlorobenzene ND 2.55 1.51 mg/Kg 59 55-103 Pentachlorophenol ND F1 5.10 ND F1 mg/Kg 6 46-115 Phenanthrene ND 2.55 1.52 mg/Kg 60 57-106 Anthracene ND 2.55 1.52 mg/Kg 60 55-105 Di-n-butyl phthalate ND 2.55 1.63 mg/Kg 64 58-109 Fluoranthene ND F1 2.55 1.41 F1 mg/Kg 53 56-104 Pyrene ND 2.55 1.62 mg/Kg 61 52-115 Butyl benzyl phthalate ND 2.55 1.80 mg/Kg 71 57-115 3,3'-Dichlorobenzidine ND 2.55 1.28 mg/Kg 50 47-110 Eurofins TestAmerica, Pleasanton Page 27 of 46 5/6/2019