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QC Sample Results Client: ProTech Consulting and Engineering Job ID: 720-92770-1 Project/Site: SRVHS Stockpile Method: 8270C - Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) (Continued) Lab Sample ID: 720-92770-5 MSD Client Sample ID: SP-1A,B,C,D Matrix: Solid Prep Type: Total/NA Analysis Batch: 265019 Prep Batch: 264883 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Hexachlorobutadiene ND 2.51 1.59 mg/Kg 63 44-110 1 35 4-Chloro-3-methylphenol ND 2.51 1.70 mg/Kg 68 58-104 1 35 2-Methylnaphthalene ND 2.51 1.51 mg/Kg 60 49-110 1 35 Hexachlorocyclopentadiene ND F1 2.51 ND F1 mg/Kg 0 24-106 NC 35 2,4,6-Trichlorophenol ND F1 2.51 0.804 F1 mg/Kg 32 50-105 25 35 2,4,5-Trichlorophenol ND F1 2.51 1.22 F1 mg/Kg 49 53-106 20 35 2-Chloronaphthalene ND 2.51 1.52 mg/Kg 61 52-110 4 35 2-Nitroaniline ND 2.51 1.56 mg/Kg 62 51-115 3 35 Dimethyl phthalate ND 2.51 1.55 mg/Kg 62 56-103 3 35 Acenaphthylene ND 2.51 1.44 mg/Kg 57 53-102 0 35 3-Nitroaniline ND 2.51 1.51 mg/Kg 60 50-110 1 35 Acenaphthene ND 2.51 1.45 mg/Kg 58 53-103 2 35 2,4-Dinitrophenol ND F1 5.02 ND F1 mg/Kg 0 10-115 NC 35 4-Nitrophenol ND F1 5.02 2.60 F1 mg/Kg 52 54-117 20 35 Dibenzofuran ND 2.51 1.44 mg/Kg 57 55-101 1 35 2,4-Dinitrotoluene ND 2.51 1.40 mg/Kg 56 54-115 0 35 2,6-Dinitrotoluene ND 2.51 1.46 mg/Kg 58 54-107 1 35 Diethyl phthalate ND 2.51 1.63 mg/Kg 65 56-107 0 35 4-Chlorophenyl phenyl ether ND 2.51 1.64 mg/Kg 65 57-106 2 35 Fluorene ND 2.51 1.43 mg/Kg 57 54-103 0 35 4-Nitroaniline ND 2.51 1.84 mg/Kg 74 49-115 0 35 2-Methyl-4,6-dinitrophenol ND F1 5.02 ND F1 mg/Kg 0 31-122 NC 35 N-Nitrosodiphenylamine ND 2.51 1.72 mg/Kg 69 56-104 5 35 4-Bromophenyl phenyl ether ND 2.51 1.64 mg/Kg 65 53-104 10 35 Hexachlorobenzene ND 2.51 1.65 mg/Kg 66 55-103 9 35 Pentachlorophenol ND F1 5.02 ND F1 mg/Kg 6 46-115 6 35 Phenanthrene ND 2.51 1.58 mg/Kg 63 57-106 4 35 Anthracene ND 2.51 1.55 mg/Kg 62 55-105 2 35 Di-n-butyl phthalate ND 2.51 1.68 mg/Kg 67 58-109 3 35 Fluoranthene ND F1 2.51 1.47 mg/Kg 57 56-104 5 35 Pyrene ND 2.51 1.57 mg/Kg 60 52-115 3 35 Butyl benzyl phthalate ND 2.51 1.79 mg/Kg 71 57-115 0 35 3,3'-Dichlorobenzidine ND 2.51 1.35 mg/Kg 54 47-110 5 35 Benzo[a]anthracene ND 2.51 1.66 mg/Kg 66 55-103 1 35 Bis(2-ethylhexyl)phthalate ND 2.51 1.92 mg/Kg 73 58-115 1 35 Chrysene ND 2.51 1.69 mg/Kg 67 58-103 3 35 Di-n-octyl phthalate ND 2.51 1.86 mg/Kg 74 58-109 3 35 Benzo[b]fluoranthene ND 2.51 1.57 mg/Kg 63 57-109 5 35 Benzo[a]pyrene ND 2.51 1.52 mg/Kg 59 57-106 1 35 Benzo[k]fluoranthene ND 2.51 1.58 mg/Kg 63 55-110 1 35 Indeno[1,2,3-cd]pyrene ND 2.51 1.50 mg/Kg 60 56-108 3 35 Benzo[g,h,i]perylene ND 2.51 1.49 mg/Kg 59 56-115 3 35 Benzoic acid ND F1 2.51 ND F1 mg/Kg 6 10-128 2 35 Pyridine ND F1 5.02 1.39 F1 mg/Kg 28 30-110 5 35 Azobenzene ND 2.51 1.51 mg/Kg 60 52-103 5 35 Dibenz(a,h)anthracene ND 2.51 1.59 mg/Kg 63 57-106 3 35 Eurofins TestAmerica, Pleasanton Page 29 of 46 5/6/2019