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QC Sample Results <br /> Client: Specialized Contracting Services Inc Job ID: 720-93292-1 <br /> Project/Site: Irby Ranch Stockpile <br /> Method: 8270C SIM - PAHs by GCMS (SIM) (Continued) <br /> Lab Sample ID: 720-93292-1 MS Client Sample ID: SP-A <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 267038 Prep Batch: 266921 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Acenaphthene ND 661 360 ug/Kg 54 46-106 <br /> Acenaphthylene ND 661 392 ug/Kg 59 46-108 <br /> Anthracene ND 661 425 ug/Kg 64 55-103 <br /> Benzo[a]anthracene ND 661 407 ug/Kg 61 54-110 <br /> Benzo[a]pyrene ND F1 661 403 F1 ug/Kg 60 62-111 <br /> Benzo[b]fluoranthene 6.0 661 452 ug/Kg 67 60-109 <br /> Benzo[g,h,i]perylene ND F1 661 187 F1 ug/Kg 28 52-114 <br /> Benzo[k]fluoranthene ND 661 431 ug/Kg 65 58-109 <br /> Chrysene ND 661 369 ug/Kg 55 54-108 <br /> Dibenz(a,h)anthracene ND F1 661 252 F1 ug/Kg 38 58-112 <br /> Fluoranthene ND F1 661 388 F1 ug/Kg 58 59-109 <br /> Fluorene ND 661 383 ug/Kg 58 52-106 <br /> Indeno[1,2,3-cd]pyrene ND F1 661 227 F1 ug/Kg 34 55-120 <br /> Naphthalene ND 661 349 ug/Kg 53 49-110 <br /> Phenanthrene ND 661 386 ug/Kg 58 57-110 <br /> Pyrene 6.9 661 547 ug/Kg 82 50-120 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 2-Fluorobiphenyl 56 33-120 <br /> Terphenyl-d 14 83 35-146 <br /> Lab Sample ID: 720-93292-1 MSD Client Sample ID: SP-A <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 267038 Prep Batch: 266921 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Acenaphthene ND 660 377 ug/Kg 57 46-106 5 35 <br /> Acenaphthylene ND 660 408 ug/Kg 62 46-108 4 35 <br /> Anthracene ND 660 426 ug/Kg 65 55-103 0 35 <br /> Benzo[a]anthracene ND 660 418 ug/Kg 63 54-110 3 35 <br /> Benzo[a]pyrene ND F1 660 415 ug/Kg 62 62-111 3 35 <br /> Benzo[b]fluoranthene 6.0 660 465 ug/Kg 70 60-109 3 35 <br /> Benzo[g,h,i]perylene ND F1 660 192 F1 ug/Kg 29 52-114 2 35 <br /> Benzo[k]fluoranthene ND 660 451 ug/Kg 68 58-109 4 35 <br /> Chrysene ND 660 378 ug/Kg 57 54-108 2 35 <br /> Dibenz(a,h)anthracene ND F1 660 260 F1 ug/Kg 39 58-112 3 35 <br /> Fluoranthene ND F1 660 394 ug/Kg 59 59-109 2 35 <br /> Fluorene ND 660 396 ug/Kg 60 52-106 3 35 <br /> Indeno[1,2,3-cd]pyrene ND F1 660 234 F1 ug/Kg 35 55-120 3 35 <br /> Naphthalene ND 660 373 ug/Kg 56 49-110 7 35 <br /> Phenanthrene ND 660 390 ug/Kg 58 57-110 1 35 <br /> Pyrene 6.9 660 552 ug/Kg 83 50-120 1 35 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 2-Fluorobiphenyl 59 33-120 <br /> Terphenyl-d14 84 35-146 <br /> Eurofins TestAmerica, Pleasanton <br /> Page 41 of 61 6/10/2019 <br />