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tan Blvd., Los Angeles, CA 90021 �' ITI VE 781 East Washington LAB SERVICE (213) 745-5312 FAX(213] 745-6372 Certificate of Analysis Page 6 of 21 File#:73101 Smith Emery Company GeoService [SF] Report Date: 04/18/19 1940 Oakdale Avenue Submitted: 04/11/19 San Francisco, CA 94124 PLS Report No.: 1904116 Attn: Mr. Patrick Morrison Phone: (800)675-8886 FAX:(415) 642-7055 Project: Seton Pacific RWC-MUUD-PHASE 1/71519-3 Sampie:ID:1A 8,,C,D Soil (1904116,011',,sampled:04/119/19 15:35 Received.04/'i1 L 09: 2 Benzo(ghi)perylene 0.0602 3 1 mg/kg 0.0500 0.200 EPA 3550C EPA 8270C 04/12/19 04/16/19 ai BD91526 r 11112-Benzo----yle- ---------------------------------------- Surrogate:2-Fluorophenol 77.2% 48-117 EPA 3550C EPA 8270C 04112119 04116119 al BD91526 Surrogate:Phenol-d5 84.7% 46-129 EPA 3550C EPA 8270C 04112119 04116119 at BD91526 Surrogate:Nitrobenzene-d5 78.3% 46-110 EPA 3550C EPA 8270C 04112119 04116119 al BD91526 Surrogate:2-Fluorobiphenyl 91.3% 49-108 EPA 3550C EPA 8270C 04112119 04116119 ai BD91526 Surrogate:2,4,6-Tribromophenol 104% 55-129 EPA 3550C EPA 8270C 04112119 04116119 ai BD91526 Surrogate:Terphenyl-dl4 145% 58-135 EPA 3550C EPA 8270C 04112119 04116119 ai BD91526 Analyte Results Flag D.F. Units MDL PQL Prep/Test Method Prepared Analyzed By Batch Naphthalene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 2-Methylnaphthalene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 1-Methylnaphthalene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Acenaphthylene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Acenaphthene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Fluorene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Phenanthrene 0.0244 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Anthracene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Fluoranthene 0.0396 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Pyrene 0.0416 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Benzo(a)anthracene 0.0207 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 (1,2-Benzanthracene) Chrysene 0.0380 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai 8091727 Benzo(b)fluoranthene 0.0234 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 (3,4-Benzofluoranthene) Benzo(k)fluoranthene 0.0170 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 (11,12-Benzofluoranthene) Benzo(a)pyrene 0.0307 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 (3,4-Benzopyrene) Indeno(1,2,3-cd)pyrene 0.0208 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 Dibenzo(a,h)anthracene ND 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 (1,2,5,6-Dibenzanthracene) Benzo(ghi)perylene 0.0247 1 mg/kg 0.0100 0.0150 EPA 3550C EPA 8270 SIM 04/12/19 04/16/19 ai BD91727 (1112_Benzo"Dfene)------------------------------------------------------------------------------------- Surrogate:Nitrobenzene-d5 86.0% 36-133 EPA 3550C EPA 8270 SIM 04112119 04116119 al BD91727 Surrogate:2-Fluorobiphenyl 771% 42-107 EPA 3550C EPA 8270 SIM 04112119 04116119 ai BD91727 Surrogate:Terphenyl--dl4 74.7% 40-149 EPA 3550C EPA 8270 SIM 04112119 04116119 ai BD91727 Analyte Results Flag D.F. Units MDL PQL Prep/Test Method Prepared Analyzed By Batch Aldrin ND 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 alpha-BHC ND 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 beta-BHC ND 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 delta-BHC ND 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 gamma-BHC(Lindane) ND 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 alpha-Chlordane 0.00279 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 gamma-Chlordane 0.00140 1 mg/kg 0.000250 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 4,4'-DDD ND 1 mg/kg 0.00100 0.00100 EPA 3550C EPA 8081A 04/15/19 04/18/19 ai BD91811 i k