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ANINk Excelchem Environmental Labs <br /> amage Environmental Project SJ County Courthouse Date Reported 01/09/06 13 24 <br /> P O Box 4869 Project Number NA <br /> Rancho Murieta CA,95683 Project Manager Joe Ramage <br /> Oxygenates - Quality Control <br /> Re o>yin S ik Sour e %REC R4 <br /> Analyte Result p Limii Units Leve Resuiit %REC Limits RPD 1 imit Notes <br /> Batch APA0024-EPA 8260B <br /> Blank(APA0024-BLKI) Prepared 01/06/06 Analyzed 01/07/06 <br /> ` Surrogate Dibromofluoromethane 125 ug/l 125 100 70-130 <br /> Surrogate Toluene-d8 124 125 992 70-130 <br /> Surrogate 4-Bromofluorobenzene 130 125 104 70-130 <br /> Ethanol ND 200 " <br /> TBA ND 50 " <br /> Methyl tert-Butyl Ether ND 05 " <br /> Di-isopropyl ether ND 05 " <br /> Ethyl Cert-Butyl Ether ND 05 " <br /> Tert-Amyl Methyl Ether ND 05 <br /> 1,2-Dichloroethane ND 05 " <br /> 1 2-Dibromoethane(EDB) ND 05 " <br /> I <br /> LCS(APA0024-BSI) Prepared 01/06/06 Analyzed 01/07/06 <br /> agate Dtbromo,Jl uoromethane 125 ug/l 125 100 70-130 <br /> ogate Toluene-d8 121 125 968 70-130 <br /> Surrogate 4-Bromofluorobenzene 133 125 106 70-130 <br /> 1,1-Dichloroethene 99 05 100 990 20-120 <br /> Benzene 98 05 100 980 20-120 <br /> Trichloroethene 93 05 too 930 20-120 <br /> Toluene 95 05 100 950 20-120 <br /> Chlorobenzene 93 05 Wo 930 20-120 <br /> I <br /> Matrix Spike(APA0024-MSI) Source 0601002-01 Prepared 01/06/06 Analyzed 01/07/06 j <br /> Surrogate Dibromofluoromethane 128 ug/1 125 102 70-130 <br /> Surrogate Toluene-d8 120 125 960 70-130 <br /> Surrogate 4-Bromofluorobenzene 129 125 103 70-130 <br /> 1,1-Dichloroethene 100 05 100 ND 100 20-120 <br /> Benzene 98 05 " 100 ND 980 20-120 <br /> Trichloroethene 94 0 5 t0 0 ND 94 0 20-120 <br /> Toluene 9 6 0 5 100 ND 960 20-120 <br /> Chlorobenzene 94 05 100 ND 94 0' 20-120 <br /> Excelchem Envirotunental Lab The results in this report apply to the samples analyzed in accordance with the chain of <br /> . custody document This analytical report must be reproduced in its entirety <br /> Laboratory Representative Page 5 of 9 <br />