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6. <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> r MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> ! htty_//www.mccaml)bell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Manteca City Corp. <br /> Date Sampled: 01/31/02 <br /> Yard Date Received: 02/01102 <br /> 837 Shaw Road <br /> Stockton,CA 95215 Client Contact: Brian Millman Date Extracted..02/07-02/11/02 <br /> Client P.O: Date Analyzed:02/07-02/11/02 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method-8260 modified <br /> Lab 1D 89494 89495 89496 89497 <br /> MW1/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client ED 01-31-02 01-31-02 01-31-02 01-31-02 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> ' Di-isopropyl Ether(DIPS) ND NO ND ND<100 5.0 1.0 i <br /> Ethyl tert-Butyl Ether(ETRE) NO NO ND ND<100 '5-0 1.0 7 <br /> :9 <br /> Methyl-tert Butyl Ether(MTBE) 7.6 6.0 NO 4200 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND NO ND ND<100 5.0 1.0 <br /> tert-Butanol ND NO ND ND<500 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 105 105 107 97 <br /> Comments: <br /> *water samples are reported in ug/.,soil and sludge sampies in ug/kg,wipes in ug/wipe and all TCLP/STLC 1SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />