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LFR INC dba LEVINE FRICKE Client Sample ID: EE-20 TOTAL Metals Lot-Sample #-__: G31)140235-007 Matrix- -- - - --: SOLID Date Sampled_ ..: 04/14/03 Date Received_ .: 04/14/03 REPORTING PREPARATION- WORK PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER " Prep Batch #_ . .. 3107333 Antimony 0.33 0.22 mg/kg SW846 6020 04/17-04/25/03 PLW251M Arsenic 6.7 0.22 mg/kg SW846 6020 04/17-04/25/03 PLW251AG Barium 177 J 0.11 mg/kg SW846 6020 04/17-04/25/03 FLW251A7 Beryllium 0.43 0.11 mg/kg SW846 6020 04/17-04/25/03 FLN251M Cadmium 0.30 0.11 mg/kg SW846 6020 04/17-04/25/03 FLW251A9 Chromium 34.0 0.22 mg/kg SW846 6020 04/17-04/25/03 FLW251CA Cobalt 10.6 0_11 mg/kg SW846 6020 04/17-04/25/03 FLW251CC Copper 59.6 J 0.22 mg/kg SW846 6020 04/17-04/25/03 FLW251CD Lead 27.0 J 0.11 mg/kg SW846 6020 04/17-04/28/03 FLW2510E Molybdenum 1.4 0.11 mg/kg SW846 6020 04/17-04/25/03 PLW251CF Nickel 38.7 J 0.22 mg/kg SW846 6020 04/17-04/25/03 FLW251CG Selenium 0.41 0.22 mg/kg SW846 6020 04/17-04/25/03 FLW251CH Silver 0.16 0.11 mg/kg SW846 6020 04/17-04/25/03 FLW251W Thallium 0.14 0.11 mg/kg SW846 6020 04/17-04/25/03 FLW251CK Vanadium 40.8 1.1 mg/kg SW846 6020 04/17-04/25/03 FLW251CL Zinc 119 J 0-55 mg/kg SW846 6020 04/17-04/25/03 FLW251f Prep Batch #. _ _: 3107495 Mercury 0.042 B 0.044 mg/kg SW846 7471A 04/17/03 PLW251CN NOTE(S) - Resulir and reporting limits Mvc been adjusred for dry Weight. J Method blenk comamioation. Tbc assodztcd mtthod bLvtk cootaiw the targe[analyte at a mponablc levet. H Evime[ed[colt Resta:u Icaa thin RL.