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LABORATORY CONTROL SAMPLE DATA REPORT <br /> GC/MS Semivolatiles <br /> Client Lot #- .. : G3E200315 Work Order #. . . : FN5LDIAC-LCS Matrix. - - - - - - - - : WATER <br /> LCS Lot-Sample#: G3E210000-397 FNSLDIAD-LCSD <br /> Prep Date. . .. . . : 05/21/03 Analysis Date. . : 05/24/03 <br /> Prep Batch #- - -: 3141397 <br /> Dilution Factor: 1 <br /> SPIKE MEASURED PERCENT <br /> PARAMETER AMOUNT AMOUNT UNITS RECOVERY RPD METHOD <br /> Acenaphthene 100 83.0 ug/L 83 SW846 8270C <br /> 100 83.2 ug/L 83 0-28 SW846 8270C <br /> 4-Chloro-3-methylphenol 100 85-9 ug/L 86 SW846 8270C <br /> 100 85.7 ug/L 86 0-25 SW846 8270C <br /> 2-Chlorophenol 100 73.8 ug/L 74 SW846 8270C <br /> 100 75.0 ug/L 75 1.7 SW846 8270C <br /> 1,4-Dichlorobenzene 100 64-9 ug/L 65 SW846 8270C <br /> 100 65.4 ug/L 65 0.73 SW846 8270C <br /> 2,4-Dini-trotoluene 100 87.6 ug/L 88 SW846 8270C <br /> 100 87.6 ug/L 88 0.040 SW846 8270C <br /> 4-91trophenol 100 42.8 ug/L 43 SW846 8270C <br /> 100 43.2 ug/L 43 0.93 SW846 8270C <br /> N-Nitrosodi-n-propyl- 100 78.0 ug/L 78 SW846 8270C <br /> amine <br /> 100 79.0 ug/L 79 1.3 SW846 8270C <br /> Pentachlorophenol 100 73.5 ug/L 74 SW846 8270C <br /> 100 76.0 ug/L 76 3-3 SW846 8270C <br /> Phenol 100 41.9 ug/L 42 SW846 8270C <br /> 100 46.2 ug/L 46 9-7 SW846 8270C <br /> Pyrene 100 88.4 ug/L 88 SW846 8270C <br /> 100 88.6 ug/L 89 0-14 SW846 8270C <br /> 1,2,4-Tr-Ichloro- 100 71.9 ug/L 72 SW846 8270C <br /> benzene <br /> 100 72.0 ug/L 72 0-15 SW846 8270C <br /> PERCENT RECOVERY <br /> SURROGATE RECOVERY LIMITS <br /> 2-Chlorophenol-d4 83 (46 - 96) <br /> 84 (46 - 96) <br /> 1,2-Dichlorobenzene-d4 68 (42 - 85) <br /> 71 (42 - 85) <br /> 2-Fluorobiphenyl 93 (50 - 101) <br /> 92 (50 - 101) <br /> 2-Fluorophenol 55 (21 - 68) <br /> 58 (21 - 68) <br /> Nitrobenzene-d5 101 (51 - 102) <br /> (Continued on next page) . <br /> G3E200315 STl Sacramento(916)373-5600 46 of 90 <br />