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MATRIX SPIES SAMPLE DATA REPORT <br /> General Chemistry <br /> Client Lot #- . . : G3E200315 Matrix. . . . . . . . . : WATER <br /> Date Sampled- - . : 05/20/03 12:35 Date Received- - : 05/20/03 15:25 <br /> SAMPLE SPIKE MEASRD PERCNT PREPARATION- PREP <br /> PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE BATCH # <br /> Chloride WO#: FN36Q1DF-MS/FN36Q1DG-MS6 MS Lot-Sample #: G3E200315-003 <br /> 173 500 673 mg/L 100 MCAWW 300.OA 05/21/03 314140: <br /> 173 500 664 mg/L 98 1.4 MCAWW 300.OA 05/21/03 3141405 <br /> Analysis Time-.: 18:35 <br /> Cyanide, Total WO#: FN36V1DD-MS/FN36V1DE-MSD MS Lot-Sample #: G3E200315-006 <br /> 0.0052 0.100 0.0878 mg/L 83 SW846 9012A 05/29-06/03/03 3149558 <br /> 0.0052 0.100 0.100 mg/L 95 13 SW846 9012A 05/29-06/03/03 314955E <br /> Analysis Time..: 20:01 <br /> Hexavalent WO#: FN34F1CJ-MS/FN34F1CK-MSD MS Lot-Sample #: G3E200315-001 i <br /> Chromium <br /> ND 0.100 0.105 mg/L 105 SW846 7196A 05/21/03 3141171 <br /> ND 0.100 0.105 mg/L 105 0.0 SW846 7196A 05/21/03 3141171 <br /> Analysis Time..: 08:30 <br /> Nitrate as N WO#: FN36QIDD-MS/FN36Q1DE-MSD MS Lot-Sample #: G3E200315-003 <br /> 0.74 ,5.00 5.46 mg/L 95 MCAWW 300.OA 05/21/03 3141404 <br /> 0.74 5.00 5.51 mg/L 96 0.87 MCAWW 300.OA 05/21/03 3141404 <br /> Analysis Time..: 19:06 <br /> Sulfate WO#: HN36Q1DH-MS/FN36QiDJ-MSD MS Lot-Sample #: G3E200315-003 <br /> 246 Soo 739 mg/L 99 MCAWW 300.OA 05/21/03 3141406 '.. <br /> 246 500 729 mg/L 97 1.4 MCAWW 300.OA 05/21/03 3141406 <br /> Analysis Time..: 18:35 <br /> Total Dissolved WO#: FN34F1DL-MS/FN34FIDM-MSD MS Lot-Sample #: G3E200315-001 <br /> Solids <br /> 657 500 1190 mg/L 106 MCAWW 160.1 05/27/03 3147306 <br /> 657 500 1210 mg/L 110 1.4 MCAWW 160.1 05/27/03 3147306 '.. <br /> Analysis Time..: 15:00 <br /> Total Organic Carbon WO#: FN34F1DN-MS/FN34FiDP-MSD MS Lot-Sample #: G3E200315-001 <br /> 0.65 10.0 10.0 mg/L 94 SW846 9060 05/29/03 3148172 <br /> 0.65 10.0 10.0 mg/L 94 0.0 SW846 9060 05/29/03 3148172 <br /> Analysis Time.. : 08:45 <br /> Total Sulfide WO#: FN34F1CQ-MS/FN34F1CR-MSD ME Lot-Sample #: G3E200315-001 <br /> ND 0.200 0.209 mg/L 104 MCAWW 376.2 05/21/03 3141409 <br /> ND 0.200 0.206 mg/L 103 1.4 MCAWW 376.2 05/21/03 3141409 <br /> Analysis Time..: 13:30 <br /> NOTE(S) : <br /> Cotculations are performed before rounding to avoid round-off cnom in ratculmd romrtm. <br /> G3E200315 STL Sacramento(916)373-5600 88 of 90 <br />