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MATRIX SPIKE SAMPLE DATA REPORT General Chemistry Client Lot #. . . : G3D220308 Matrix. . - - - - . . . . WATER Date Sampled. . . : 04/17/03 10:35 Date Received. . : 04/17/03 13:55 SAMPLE SPIKE MFASRD PERCNT PREPARATION- PREP PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE BATCH # Chloride WO#: FMD831CK-MS/FMD831CL-MSD MS Lot-Sample #: G3D220308-001 164 200 358 mg/L 97 MCAWW 300. OA 04/22/03 311249' 164 200 356 mg/L 96 0.63 MCAWW 300.OA 04/22/03 3112497 Analysis Time-.: 18:02 Cyanide, Total WO#: FMD831Cl-MS/FM831C2-MSD MS Lot-Sample #: G3D220308-001 ND - 0.200 0.203 mg/L 101 SW846 9012A 04/29-05/03/03 3119544 ND 0.200 0.197 mg/L 99 2.6 SW846 9012A 04/29-05/03/03 3119544 Analysis Time..: 15:02 Hexavalent WO#: FMD831CX-MS/FMD831CO-MSD MS Lot-Sample #: G3D220308-001 Chromium ND 0.100 0.105 mg/L 105 SW846 7196A 04/22/03 3112546 ND 0.100 0.100 mg/L 100 4.9 SW846 7196A 04/22/03 3112546 Analysis Time..: 17:30 Nitrate as N WO#v FMD831CM-MS/FMD831CN-MSD MS Lot-Sample #: G3D220308-001 5.2 20.0 24.6 mg/L 97 MCAWW 300.OA 04/22/03 3112549 5.2 20.0 24.4 mg/L 96 0.73 MCAWW 300.OA 04/22/03 3112549 Analysis Time..: 18:02 Sulfate WO#: FMD831CP-MS/FMD831CQ-MSD MS Lot-Sample #: G3D220308-001 142 200 343 mg/L 101 MCAWW 300.OA 04/22/03 3112550 142 200 337 mg/L 98 1.8 MCAWW 300.OA 04/22/03 3112550 Analysis Time..: 18:02 Total Dissolved WO#: FL53AlAL-MS/FL53AIAM-MSD MS Lot-Sample #: G3D170303-001 Solids 293 500 777 mg/L 97 MCAWW 160.1 04/23/03 3113594 293 500 815 mg/L 104 4.8 MCAWW 160.1 04/23/03 3113594 Analysis Time..: 18:30 Total Sulfide WO#: FLGGKIAF-MS/FL6GKIAG-MSD MS Lot-Sample #: G3D170355-001 ND 0.200 0.109 N mg/L 54 MCAWW 376.2 04/23/03 3113149 ND 0.200 0.119 N mg/L 60 8.8 MCAWW 376.2 04/23/03 3113149 Analysis Time..: 12:30 NOTE(S) : Calculations are performed before rounding to avoid round-off errors in calculated revults. N Spiked analyte recovery is outside stated control limits. G30220308 STL-Sacramento(916)373-5600 59 of 61