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MATRIX SPIKE SAMPLE EVALUATION REPORT <br /> € DISSOLVED Metals <br /> Client Lot #. .. : G3,3'090369 <br /> Matrix,. ... . WA'T'ER <br /> Date Sampled___ : 10/09/03 Date Received. .: 10/09/03 <br /> PERCENT RECOVERY RPD <br /> PARAMETER _ RECOVERY LIMI'T'S RPD LIMITS METHOD PREPARAT3ON WORK <br /> ANALYSIS DATE ORDER # <br /> MS Lot-Sample #: G3J090369-001 Prep Batch #...: 3286414 <br /> Aluminum 104 (91 - 120) SW846 6020 10/13-10/31/03 F18DA1C3 <br /> 109 (91 - 320) 4.2 (0-15) SW846 6020 10/13-10/31/03 F18DA1C4 <br /> Antimony 100 (91 - 111) SW846 6020 10/13-10/31/03 FISDAIC5 <br /> 99 (91 - 111) 0.85 (0-15) SW846 6020 10/13-10/31/03 F18DAIC6 <br /> Arsenic 100 (89 - 109) SW846 6020 10/13-10/31/03 F18DA1C7 <br /> 100 (89 - 109) 0.25 (0-15) SW846 6020 10/13-10/31/03 F18DA7;C8 <br /> Barium 94 (89 - 111) SW846 6020 10/23-10/31/03 F18DA1C9 <br /> 94 (89 - 111) 0.22 (0-15) SW846 6020 10/13-10/31/03 F18DA1DA <br /> Beryllium 99 (86 - 1ZZ) SW846 6020 10/13-10/31/03 F18DA1DC <br /> 9$ (86 _ 311) 0.35 (0-15) SW846 6020 10/13-10/31/03 F18DA1DD <br /> Cadmium 91 (90 - 110) SW846 6020 10/13-10/31/03 F18DA1DE <br /> 90 (90 - 110) 0.73 (0-15) SW846 6020 10/13-10/31/03 F18DA1DF <br /> Calcium NC,MSB (92 - 125) SW846 6020 10/13-10/31/03 F18DAIDG <br /> NC,MSB (92 - 125) {p-15) SW846 6020 7.0/13-10/31/03 FISDA1DH <br /> Chromium 100 (87 - 120) SW846 6020 10/13-10/31/03 F18DA1D,T <br /> <- 100 (87 - 120) 0.93 (0-15) SW846 6020 10/13-10/31/03 P18DAIDK <br /> d._ Cobalt 102 (89 - 120) SW846 6020 10/13-10/31/03 F18DA1DL <br /> 102 (89 - 120) 0.51 (0..15) SW846 6020 10/13-10/31/03 F18DA1DM <br /> Copper 94 (92 - 113) SW846 6020 10/13-10/31/03 F18DA1DN <br /> ..,. 94 (92 - 113) 0.34 (0-15) SW846 6020 10/13-10/31/03 F1SDA1Dp <br /> Iron 105 (88 - 119) SW846 6020 10/13-10/31./03 F18DAIDQ <br /> 108 (88 - 119) 2.6 (0-15) SW846 6020 10/3.3-10/31/03 F1SDAIDR <br /> Lead 97 (88 - 121) SW846 6020 10/13-10/31/03 F18DAIDT <br /> 96 (88 - 123) 0.90 (0-15) SW846 6020 10/13-10%31/03 F18DA1DU <br /> Magnesium NC,MSB (93 - 115) SW846 6020 10/13-10/31/03 F18DAI.DV <br /> NC,MSB (93 - 115) (0-15) SW846 6'020 10/13--10/31/03 FISDAIDw <br /> Manganese 99 (87 - 123) SW846 6020 10/13-10/31/03 F18DAlDX <br /> 101 (87 - 123) 2.3 (0-15) SW846 6020 10/13-10/31/03 F18DAJDO <br /> Nickel 95 (93 - 113) SW846 6020 3.0/13-.10/31/03 P18DAIDI <br /> 95 (93 - 113) 0.45 (0-15) SW846 6020 10/13-10/31/03 F18DAZD2 <br /> Y Potassium NC,MSB (92 - 118) SW846 6020 10/13-10/31/03 F18DA1D3 <br /> NC,MSB (92 - 1.18) (0-17) SW846 6020 10/13-10/3.1/03 F18DA1D4 <br /> Selenium 99 (89 - 110) SW846 6020 10/13-10/31/03 FISDA1D5 <br /> ' 100 (89 - 110) 1.4 (0-15) SW846 6020 10/13-10/31/03 F1SDA1D6 <br /> Silver 87 N (90 - 112) SW846 6020 10/3.3-10/31/03 F18DA1D7 <br /> 87 N (90 - 112) 0.40 (0-15) SW846 6020 10/13-10/31/03 F18DA11M8 <br /> Sodium NC,MSB (90 - 320) SW846 6020 10/13-10/31/03. F18DA1D9 <br /> NC,MSB (90 - 120) (0-15) SW846 6020 10/13-10/31J03 F18DAlEA <br /> m- Thallium 93 (87 - 119) SW846 6020 10/13-10/31/03 F1SDAIEC <br /> 92 (87 - 119) 1.1 (0-15) SW846 6020 10/13-10/31/03 F18DAIED <br /> Tin 99 (86 - 112) SW846 6020 10/13-10/31/03 P18DAIEE <br /> 99 (86 - 132) 0.10 (0-15) SW846 6020 10/13-10/31/03 F18DAJEF <br /> (Continued on next page) <br /> k--90369 STL Sacramento 916373-5600 <br /> • 65 of 96 <br />