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I <br /> Ameru an Ent rrnn/nental NeAvork <br /> WORK ORDER 9803x39 QUALITY CONTROL REPORT PAGE QR-6 <br /> . ANALYSIS Volatile GUMS <br /> MATRIX- Water <br /> METHOD BLANK SAMPLES <br /> -- -- ----- ------ - - - - <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 0311 INSTR RUN GCMS121980311000000/1/ <br /> f INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12WO31198 <br /> UNITS ug/L ANALYZED 03/11/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORT;NG SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMI VALUE (X) LOW HIGH RPD (X) LIMIT (t) <br /> trans 1 4 DZchloro 2 buten NO 100 <br /> cis 1 3 Dichloropropene NO 5 <br /> E trans 1 3 Dichloropropene ND 5 <br /> 2 Hexanone ND 50 <br /> Methyl Iodide ND 200 <br /> 4 Methyl 2 pentanone ND 50 <br /> Vinyl Acetate ND 50 <br /> 2 Chloroethyl Vinyl Ether NO 10 <br /> MTBE NO 5 <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 0313 INSTR RUN GCMS121980313000000/l/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED — BATCH ID MS12W131398 <br /> UNITS ug/L ANALYZED 03/13/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (t) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCA d4 (surr) 117 100 65 135 <br /> E Toluene d8 (surr) 96 6 100 70 130 <br /> p BFB (surr) 108 100 70 130 <br /> I 1 Ozchloroethene NO E <br /> Benzene ND 5 <br /> Trichloroethene NO E <br /> Toluene NO <br /> Chlorobenzene NO <br /> Acetone ND 101 <br /> f Bromodichloromethane ND 5 <br /> Bromoform ND E <br /> Bromomethane NO 1C <br /> 2 Butanone ND 10C <br /> Carbon Disulfide ND IC <br /> Carbon Tetrachloride ND E <br /> Chloroethane ND 1C <br /> 2 Chloroethyl Vinyl Ether ND iC <br /> Chloroform ND 5 <br /> Chloromethane NO 1C <br /> Dibromochloromethane ND 5 <br /> 1 1 Dichloroethane ND 5 <br /> l 1 2 Dichloroethane NO 5 <br /> f cis 1 2 Dichloroethene NO 5 <br /> 4 trans 1 2 Dichloroethene NO 5 <br /> 1 2 Dichloropropane NO 5 <br /> cis 1 3 Dichloropropene NO 5 <br /> 4 trans 1 3 Dichloropropene ND 5 <br /> Ethylbenzene ND 5 <br /> 2 Hexanone NO 50 <br /> Methylene Chloride ND 10 <br /> 4 Methyl 2 pentanone ND 50 <br /> Styrene ND 5 <br /> 1 1 2 2 Tetrachloroethane ND 5 <br /> Tetrachloroethene ND 5 <br /> 1 1 1 Trichloroethane ND 5 <br /> 1 1 2 Trichloroethane ND 5 <br /> Vinyl Acetate ND 50 <br /> Vinyl Chloride ND 10 <br /> Xylenes Total ND 10 <br /> 1 2 Dibromoethane ND 5 <br /> 1 2 Dichlorobenzene NO 5 <br /> 1 3 Dichlorobenzene NO 5 <br /> 1 4 Dichlorobenzene NO 5 <br /> Dichlorodifluoromethane NO 10 <br /> Trichlorofluoromethane NO 5 <br /> Trichlorotrifluoroethane ND 5 <br /> Tetrahydrofuran NO 50 <br />